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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R040059
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.034
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   18.9210 4.694727   0 -2  2    2   18.9308  4.692317    0.0098  0.002410
   22.0091 4.041467  -2  0  2    2   22.0091  4.041471    0.0000 -0.000004
   23.5327 3.782760  -1  3  0    2   23.5306  3.783094   -0.0021 -0.000334
   24.6012 3.620602   1  3  0    2   24.6049  3.620067    0.0037  0.000535
   26.5071 3.364104  -1  1  4    2   26.5136  3.363294    0.0065  0.000810
   27.3560 3.261477  -2  2  0    2   27.3437  3.262923   -0.0123 -0.001446
   28.5825 3.124084   2  2  0    2   28.5890  3.123382    0.0065  0.000702
   30.2724 2.953228   0 -4  2    2   30.2743  2.953050    0.0019  0.000179
   30.4490 2.936482   0 -2  4    2   30.4484  2.936537   -0.0006 -0.000055
   30.9008 2.894522  -2 -2  4    2   30.9009  2.894515    0.0001  0.000007
   31.6515 2.827488   1  3  2    2   31.6462  2.827952   -0.0053 -0.000464
   31.9095 2.805188  -1 -3  4    2   31.9034  2.805709   -0.0061 -0.000521
   41.5103 2.175343  -3  3  0    2   41.5115  2.175282    0.0012  0.000060
   42.1349 2.144503   2 -4  2    2   42.1369  2.144404    0.0020  0.000099
   43.1762 2.095123   1  5  2    2   43.1756  2.095151   -0.0006 -0.000028
   50.6735 1.801118  -1  7  0    2   50.6738  1.801109    0.0003  0.000008

 rmse = 0.00004291048
 
     A =     8.182(1)          B =    12.8751(9)          C =    14.177(2)       
 Alpha =    93.21(1)        Beta =   115.84(1)        Gamma =    91.20(1)        
 
 Volume =   1340.3(2)