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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050107
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.018
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   11.5245 7.683838  -2  0  2    2   11.5244  7.683878   -0.0001 -0.000039
   13.7320 6.451581   2  1  1    2   13.7257  6.454519   -0.0063 -0.002939
   15.1069 5.866675   2  0  2    2   15.1067  5.866767   -0.0002 -0.000092
   17.6145 5.035897   0  2  0    2   17.6190  5.034616    0.0045  0.001282
   19.5448 4.542223   4  1  1    2   19.5475  4.541606    0.0027  0.000617
   26.3208 3.385444   6  1  1    2   26.3223  3.385254    0.0015  0.000190
   27.7591 3.213100  -2  3  1    2   27.7572  3.213313   -0.0019 -0.000213
   27.9826 3.187926   6  0  2    2   27.9785  3.188383   -0.0041 -0.000457
   29.2285 3.054727  -4  2  4    2   29.2333  3.054232    0.0048  0.000494
   31.2987 2.857121  -2  3  3    2   31.2960  2.857358   -0.0027 -0.000236
   32.4703 2.756599  -2  0  6    2   32.4685  2.756745   -0.0018 -0.000146
   33.2498 2.693699   6  2  2    2   33.2503  2.693657    0.0005  0.000042
   35.4008 2.534717   4  2  4    2   35.4031  2.534556    0.0023  0.000160
   36.9137 2.434181  -8  2  4    2   36.9132  2.434214   -0.0005 -0.000033

 rmse = 0.00002085453
 
     A =    24.672(2)          B =    10.0692(8)          C =    16.573(1)       
 Alpha =    90.             Beta =   106.534(5)       Gamma =    90.             
 
 Volume =   3947.2(3)