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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050423
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.051
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   14.9751 5.931202   0  1  1    2   14.9790  5.929679    0.0039  0.001523
   26.5026 3.366774   1  0  2    2   26.5024  3.366803   -0.0002 -0.000029
   37.7464 2.384376   0  0  4    2   37.7409  2.384711   -0.0055 -0.000336
   39.6357 2.274818   0  1  4    2   39.6411  2.274522    0.0054  0.000296
   43.9527 2.060617  -1  1  4    2   43.9525  2.060623   -0.0002 -0.000007
   48.0867 1.892484   0  4  0    2   48.0859  1.892514   -0.0008 -0.000030
   65.3448 1.427874  -1  5  1    2   65.3450  1.427870    0.0002  0.000004

 rmse = 0.00004196970
 
     A =     4.790(2)          B =     7.5700(4)          C =     9.5391(8)      
 Alpha =    90.             Beta =    90.44(1)        Gamma =    90.             
 
 Volume =    345.9(1)