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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 R050288
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.020
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   11.3554 7.799666   1  0  0    2   11.3640  7.793787    0.0086  0.005879
   15.4557 5.735767  -1  0  1    2   15.4555  5.735829   -0.0002 -0.000062
   22.0851 4.025170   0  1  1    2   22.0767  4.026691   -0.0084 -0.001520
   22.9998 3.866977  -1  1  1    2   22.9929  3.868122   -0.0069 -0.001145
   23.2633 3.823731  -2  0  1    2   23.2781  3.821332    0.0148  0.002399
   27.4659 3.247025  -1  0  2    2   27.4586  3.247875   -0.0073 -0.000850
   28.3541 3.147225   0  0  2    2   28.3515  3.147504   -0.0026 -0.000279
   28.5498 3.126080   2  1  0    2   28.5442  3.126679   -0.0056 -0.000599
   30.1231 2.966185   2  0  1    2   30.1275  2.965759    0.0044  0.000426
   33.4575 2.677623  -3  0  1    2   33.4594  2.677472    0.0019  0.000152
   34.2215 2.619538   0  2  0    2   34.2245  2.619311    0.0030  0.000227
   34.7570 2.580371   2  1  1    2   34.7501  2.580866   -0.0069 -0.000495
   35.6854 2.515301  -2  1  2    2   35.6809  2.515610   -0.0045 -0.000309
   36.1603 2.483330   1  2  0    2   36.1676  2.482846    0.0073  0.000485
   41.7959 2.160428  -2  2  1    2   41.7946  2.160493   -0.0013 -0.000065
   42.9037 2.107148  -2  0  3    2   42.8968  2.107471   -0.0069 -0.000323
   44.4085 2.039143  -1  2  2    2   44.4143  2.038888    0.0058  0.000255
   44.7164 2.025809   3  1  1    2   44.7238  2.025491    0.0074  0.000318
   46.2269 1.963040   2  2  1    2   46.2217  1.963249   -0.0052 -0.000209
   51.4175 1.776319   3  0  2    2   51.4171  1.776332   -0.0004 -0.000013
   54.5081 1.682641   0  3  1    2   54.5071  1.682668   -0.0010 -0.000027
   57.6308 1.598638  -4  1  3    2   57.6339  1.598560    0.0031  0.000078
   59.0665 1.563146   4  2  0    2   59.0585  1.563340   -0.0080 -0.000194
   63.2045 1.470366   3  2  2    2   63.2150  1.470147    0.0105  0.000219
   66.1641 1.411565   1  1  4    2   66.1640  1.411568   -0.0001 -0.000002
   71.2322 1.323032  -4  3  1    2   71.2384  1.322932    0.0062  0.000099
   77.6322 1.229133   4  3  1    2   77.6243  1.229239   -0.0079 -0.000106

 rmse = 0.00006446528
 
     A =8.1118(6)              B =5.2386(3)               C =6.5519(4)           
 Alpha =90                  Beta =106.097(5)          Gamma =90                  
 
 Volume = 267.50(2)