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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070168
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.030
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   11.3910 7.782007   1  1  0    2   11.3990  7.776574    0.0080  0.005434
   12.3959 7.151785  -1  1  1    2   12.3993  7.149799    0.0034  0.001986
   14.8753 5.962443   1  1  1    2   14.8777  5.961470    0.0024  0.000973
   15.1729 5.845929   0  0  2    2   15.1718  5.846354   -0.0011 -0.000426
   15.5852 5.691895   2  0  0    2   15.5856  5.691742    0.0004  0.000153
   16.6733 5.322145   0  2  0    2   16.6663  5.324360   -0.0070 -0.002215
   17.1161 5.185203  -1  1  2    2   17.1214  5.183596    0.0053  0.001607
   18.3241 4.845447   0  2  1    2   18.3234  4.845636   -0.0007 -0.000189
   26.3073 3.388689   1  3  0    2   26.3076  3.388654    0.0003  0.000035
   26.7736 3.330653  -1  3  1    2   26.7686  3.331267   -0.0050 -0.000615
   29.1139 3.067749  -2  2  3    2   29.1119  3.067960   -0.0020 -0.000211
   31.4354 2.846073   4  0  0    2   31.4377  2.845871    0.0023  0.000202
   31.6283 2.829137   1  3  2    2   31.6259  2.829350   -0.0024 -0.000213
   33.6697 2.661974   0  4  0    2   33.6670  2.662180   -0.0027 -0.000206
   34.8347 2.575492   1  1  4    2   34.8297  2.575850   -0.0050 -0.000358
   35.0162 2.562546  -3  3  2    2   35.0240  2.561994    0.0078  0.000552
   36.5806 2.456376   1  3  3    2   36.5857  2.456048    0.0051  0.000328
   38.6211 2.331061  -2  4  2    2   38.6255  2.330804    0.0044  0.000257
   40.7311 2.214952   3  3  2    2   40.7285  2.215087   -0.0026 -0.000134
   42.1310 2.144484   2  2  4    2   42.1338  2.144348    0.0028  0.000136
   44.3530 2.041996   1  5  1    2   44.3495  2.042147   -0.0035 -0.000152
   47.5720 1.910972  -5  3  3    2   47.5688  1.911093   -0.0032 -0.000121
   61.4698 1.507864   1  7  0    2   61.4708  1.507841    0.0010  0.000022

 rmse = 0.00003103454
 
     A =11.8774(9)             B =10.6487(3)              C =12.200(1)           
 Alpha =90                  Beta =106.581(7)          Gamma =90                  
 
 Volume = 1478.9(1)