Boulangerite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern for R050441 Skowron A, Brown I D Acta Crystallographica C46 (1990) 531-534 Refinement of the structure of boulangerite, Pb5Sb4S11 CELL PARAMETERS: 23.48798 21.19124 4.039659 90.00000 90.00000 90.00000 SPACE GROUP: Pnam X-RAY WAVELENGTH: 1.541838 2-THETA INTENSITY D-SPACING H K L 11.34 4.20 7.8670 2 2 0 13.18 6.66 6.7645 1 3 0 14.73 8.65 6.0532 2 3 0 17.25 1.19 5.1680 1 4 0 18.46 3.81 4.8292 2 4 0 19.44 5.75 4.5863 5 1 0 20.33 8.39 4.3877 3 4 0 21.39 1.46 4.1709 1 5 0 22.39 7.86 3.9866 2 5 0 22.49 8.18 3.9682 0 1 1 22.69 7.58 3.9335 4 4 0 22.80 4.82 3.9147 6 0 0 22.82 23.83 3.9116 5 3 0 22.81 23.24 3.9128 1 1 1 23.19 21.22 3.8495 6 1 0 23.75 11.43 3.7594 2 1 1 23.96 100.00 3.7272 3 5 0 23.96 78.06 3.7268 1 2 1 24.32 34.01 3.6721 6 2 0 24.86 1.40 3.5936 2 2 1 25.30 1.48 3.5319 0 6 0 25.48 7.49 3.5067 0 3 1 25.77 10.00 3.4683 1 3 1 26.01 12.11 3.4366 4 5 0 26.61 9.13 3.3601 2 3 1 26.98 33.50 3.3141 7 1 0 27.79 39.77 3.2195 3 6 0 27.97 3.80 3.1989 7 2 0 27.96 20.24 3.2004 3 3 1 28.12 5.79 3.1827 1 4 1 29.59 28.76 3.0266 4 6 0 29.55 8.48 3.0314 5 1 1 29.75 64.49 3.0107 4 3 1 30.15 24.82 2.9719 3 4 1 30.46 10.90 2.9424 5 2 1 30.89 2.34 2.9018 1 5 1 31.61 14.96 2.8375 2 5 1 31.70 6.28 2.8294 8 2 0 31.77 32.32 2.8236 3 7 0 31.83 53.24 2.8182 4 4 1 31.91 40.71 2.8112 6 0 1 31.92 2.22 2.8101 5 3 1 32.20 83.36 2.7868 6 1 1 32.77 1.44 2.7393 3 5 1 33.04 17.10 2.7172 6 2 1 33.37 21.57 2.6908 4 7 0 33.88 14.61 2.6516 5 4 1 34.66 2.59 2.5933 2 6 1 34.79 7.24 2.5840 2 8 0 35.01 1.19 2.5680 8 4 0 35.74 9.16 2.5177 3 6 1 35.86 1.72 2.5092 3 8 0 36.26 1.19 2.4825 5 5 1 36.78 4.66 2.4480 9 3 0 37.16 18.22 2.4244 7 3 1 37.39 1.80 2.4098 1 7 1 37.99 39.10 2.3726 2 7 1 38.49 4.87 2.3428 1 9 0 38.52 12.60 2.3411 9 4 0 38.50 4.90 2.3427 6 5 1 38.88 4.70 2.3204 7 4 1 39.09 1.81 2.3086 2 9 0 38.93 12.96 2.3175 8 2 1 38.99 1.01 2.3143 3 7 1 39.11 2.05 2.3074 5 8 0 40.12 22.01 2.2512 8 3 1 40.34 1.69 2.2395 4 7 1 40.67 4.01 2.2223 9 5 0 40.99 4.19 2.2054 1 8 1 41.55 15.02 2.1768 2 8 1 42.03 7.40 2.1531 5 7 1 42.15 19.42 2.1472 10 4 0 42.48 5.07 2.1315 3 8 1 42.73 2.40 2.1191 0 10 0 43.04 1.33 2.1050 5 9 0 43.16 1.48 2.0989 9 6 0 43.74 2.96 2.0726 4 8 1 44.15 9.78 2.0544 10 5 0 44.38 2.84 2.0439 11 3 0 44.61 10.86 2.0343 0 9 1 44.81 2.21 2.0256 9 4 1 44.94 45.33 2.0198 0 0 2 45.30 2.14 2.0044 2 9 1 45.32 8.37 2.0036 5 8 1 45.55 5.00 1.9942 10 2 1 45.98 1.80 1.9767 9 7 0 46.12 1.24 1.9708 8 6 1 46.22 3.62 1.9667 8 8 0 46.45 1.62 1.9573 12 0 0 47.11 1.51 1.9317 5 10 0 47.20 2.72 1.9279 6 8 1 47.29 2.17 1.9248 12 2 0 47.41 3.90 1.9200 1 11 0 47.35 14.28 1.9222 4 9 1 48.74 1.23 1.8707 3 11 0 48.74 8.03 1.8706 1 10 1 48.79 1.11 1.8686 8 7 1 48.85 2.60 1.8667 5 9 1 48.93 9.70 1.8636 6 10 0 48.96 45.18 1.8625 9 6 1 49.15 1.93 1.8557 10 7 0 49.08 7.20 1.8585 11 2 1 49.35 2.43 1.8486 7 8 1 49.72 1.17 1.8360 12 4 0 49.86 2.65 1.8312 10 5 1 49.75 1.09 1.8348 3 4 2 50.04 1.35 1.8249 3 10 1 50.07 1.38 1.8238 11 3 1 50.72 1.43 1.8018 2 5 2 50.88 1.35 1.7968 4 4 2 50.93 1.10 1.7950 6 0 2 50.94 4.58 1.7947 5 3 2 51.12 3.90 1.7886 6 1 2 51.36 3.60 1.7811 13 2 0 51.83 7.15 1.7659 0 12 0 51.52 20.26 1.7758 3 5 2 51.98 1.97 1.7610 1 12 0 51.71 6.96 1.7698 6 2 2 51.97 4.83 1.7615 12 0 1 52.00 5.94 1.7603 10 6 1 52.10 6.40 1.7574 10 8 0 52.16 8.01 1.7554 12 1 1 52.32 6.76 1.7504 13 3 0 52.50 3.65 1.7449 11 7 0 52.57 1.79 1.7427 5 10 1 52.67 2.31 1.7395 7 9 1 52.85 5.28 1.7341 1 11 1 52.61 2.35 1.7413 4 5 2 53.03 7.46 1.7285 6 11 0 53.17 1.08 1.7245 11 5 1 53.16 7.94 1.7248 7 1 2 53.62 9.43 1.7110 3 6 2 54.68 7.22 1.6801 4 6 2 55.02 1.40 1.6707 7 11 0 54.96 1.20 1.6721 8 9 1 54.95 2.65 1.6725 14 1 0 55.51 4.88 1.6571 14 2 0 55.65 1.02 1.6530 5 12 0 55.99 2.06 1.6439 8 2 2 56.03 9.75 1.6428 3 7 2 56.48 1.22 1.6307 5 11 1 57.06 6.49 1.6154 4 7 2 58.09 7.77 1.5891 6 11 1 58.00 2.67 1.5913 2 8 2 59.37 1.92 1.5580 9 3 2 59.96 1.69 1.5439 7 11 1 60.57 3.82 1.5299 5 12 1 60.57 1.91 1.5298 1 9 2 60.59 4.99 1.5293 9 4 2 61.67 1.64 1.5052 12 9 0 61.93 2.45 1.4993 2 13 1 62.15 1.96 1.4947 9 5 2 62.50 2.72 1.4871 14 4 1 63.17 1.08 1.4729 11 9 1 63.49 3.61 1.4662 7 13 0 63.25 8.40 1.4712 10 4 2 63.69 1.22 1.4621 0 10 2 64.02 1.52 1.4552 14 5 1 64.08 1.26 1.4541 16 2 0 64.37 2.15 1.4483 13 7 1 64.83 2.39 1.4390 5 13 1 64.92 1.19 1.4373 16 3 0 64.77 4.53 1.4403 10 5 2 65.12 1.26 1.4334 13 9 0 64.95 1.42 1.4367 11 3 2 65.54 1.86 1.4252 8 13 0 66.08 5.59 1.4148 1 14 1 66.32 2.04 1.4102 6 13 1 66.35 2.59 1.4096 11 10 1 66.19 1.04 1.4127 9 7 2 66.48 2.16 1.4072 2 14 1 66.46 5.28 1.4075 15 4 1 66.38 1.95 1.4091 8 8 2 67.15 1.05 1.3948 3 14 1 67.22 1.27 1.3934 12 2 2 67.32 1.98 1.3916 1 11 2 67.98 1.37 1.3798 7 14 0 67.94 2.84 1.3804 15 5 1 68.01 1.84 1.3793 14 7 1 68.55 5.43 1.3697 6 10 2 69.78 1.86 1.3483 11 11 1 70.44 2.75 1.3374 14 8 1 70.53 2.01 1.3359 13 2 2 70.92 4.18 1.3295 0 12 2 70.66 2.29 1.3337 1 2 3 71.05 1.15 1.3273 1 12 2 71.14 3.73 1.3258 10 8 2 71.33 3.98 1.3228 13 3 2 71.48 2.19 1.3204 11 7 2 72.06 1.56 1.3112 12 12 0 71.93 4.40 1.3133 6 11 2 72.01 2.37 1.3120 16 5 1 72.41 1.02 1.3057 7 14 1 72.47 1.64 1.3048 17 1 1 72.78 5.18 1.3000 12 11 1 73.55 1.70 1.2882 14 1 2 73.41 2.83 1.2904 4 3 3 73.61 1.39 1.2873 3 4 3 74.03 3.16 1.2811 14 2 2 74.51 2.38 1.2740 4 4 3 74.55 1.63 1.2733 6 0 3 74.71 4.68 1.2710 6 1 3 75.80 2.28 1.2555 16 7 1 76.39 2.81 1.2471 12 12 1 76.72 1.45 1.2426 3 16 1 76.94 1.83 1.2396 2 17 0 76.94 2.17 1.2396 18 1 1 77.57 1.59 1.2310 3 17 0 77.41 1.74 1.2333 18 2 1 77.61 1.51 1.2306 4 16 1 77.61 1.12 1.2306 7 3 3 78.13 2.56 1.2236 2 7 3 78.86 3.50 1.2142 8 15 1 79.55 1.10 1.2054 13 12 1 79.42 1.25 1.2069 12 9 2 79.50 1.68 1.2060 8 3 3 80.65 1.95 1.1916 17 9 0 80.44 1.34 1.1941 2 8 3 81.06 2.69 1.1866 7 13 2 82.05 1.84 1.1748 19 2 1 82.55 1.13 1.1689 0 9 3 82.93 1.49 1.1645 8 13 2 84.52 1.11 1.1466 20 4 0 84.53 1.60 1.1464 4 9 3 85.18 1.12 1.1393 7 14 2 85.74 5.31 1.1334 9 6 3 88.20 1.09 1.1079 12 1 3 89.02 1.51 1.0998 12 12 2 89.02 1.51 1.0998 12 12 2 XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.