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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 file_id=6989[1]
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.019
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   65.6504 1.421338   0  0 10    2   65.6495  1.421356   -0.0009 -0.000018
   45.2360 2.003672  -1  3  5    2   45.2360  2.003672    0.0000  0.000000
   44.6021 2.030678   0  0  7    2   44.6060  2.030509    0.0039  0.000169
   36.8329 2.439400  -2  0  3    2   36.8329  2.439400    0.0000  0.000000
   31.4646 2.842512   0  0  5    2   31.4623  2.842713   -0.0023 -0.000201
   25.0600 3.553097   0  0  4    2   25.0579  3.553391   -0.0021 -0.000294
   23.0667 3.855678   0  2  2    2   23.0667  3.855678    0.0000  0.000000
   18.7331 4.737598   0  0  3    2   18.7321  4.737855   -0.0010 -0.000256
   12.4651 7.105790   0  0  2    2   12.4634  7.106782   -0.0017 -0.000992
    6.227114.224426   0  0  1    2    6.2318 14.213564    0.0047  0.010863

 rmse = 0.00001989057
 
     A =5.305(1)               B =9.180(2)                C =14.339(1)           
 Alpha =90                  Beta =97.57(3)            Gamma =90                  
 
 Volume = 692.2(3)