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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R040122
 
 Symmetry constraint is: MONOCLINIC3 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.096
  
 Number of iterations =   4

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   17.7120 5.030564   0 -2  1    2   17.7170  5.029153    0.0050  0.001411
   23.0452 3.872122   1  0  2    2   23.0559  3.870342    0.0107  0.001780
   25.6220 3.486773   1  1  2    2   25.6182  3.487282   -0.0038 -0.000509
   32.4334 2.766188   1 -3  1    2   32.4265  2.766763   -0.0069 -0.000575
   34.4871 2.605554   1  3  1    2   34.4979  2.604765    0.0108  0.000790
   35.3815 2.541531   1  1  4    2   35.3706  2.542290   -0.0109 -0.000758
   37.4142 2.407630   1  3  2    2   37.4119  2.407771   -0.0023 -0.000141
   38.2276 2.358121   1 -1  5    2   38.2208  2.358529   -0.0068 -0.000408
   42.0006 2.154107   2  1  2    2   42.0093  2.153678    0.0087  0.000429
   54.1463 1.695242   1 -3  7    2   54.1492  1.695159    0.0029  0.000083
   55.5097 1.656715   2 -3  5    2   55.5070  1.656789   -0.0027 -0.000073
   62.4445 1.488065   0  0  9    2   62.4462  1.488029    0.0017  0.000036
   68.1795 1.376008   3  3  2    2   68.1783  1.376030   -0.0012 -0.000021

 rmse = 0.00006572154
 
     A =     4.7428(4)         B =    10.239(2)           C =    13.6355(8)      
 Alpha =   100.83(1)        Beta =    90.             Gamma =    90.             
 
 Volume =    650.4(1)