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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R061103
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.027
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    6.271214.142567   0  0  2    2    6.2781 14.126984    0.0069  0.015583
   12.5496 7.062626   0  0  4    2   12.5481  7.063492   -0.0015 -0.000865
   18.8586 4.708334   0  0  6    2   18.8559  4.708995   -0.0027 -0.000660
   25.2243 3.531428   0  0  8    2   25.2220  3.531746   -0.0023 -0.000318
   28.5428 3.127558  -1  1  7    2   28.5424  3.127606   -0.0004 -0.000048
   31.6688 2.825344   0  0 10    2   31.6682  2.825397   -0.0006 -0.000053
   35.8976 2.501365   2  0  4    2   35.8977  2.501360    0.0001  0.000005
   38.2216 2.354341   0  0 12    2   38.2190  2.354497   -0.0026 -0.000156
   40.3514 2.234769   0  2 11    2   40.3514  2.234769    0.0000  0.000000
   46.4066 1.956122  -1  3 10    2   46.4069  1.956109    0.0003  0.000013
   66.1050 1.412813   0  0 20    2   66.1110  1.412698    0.0060  0.000114
   72.3358 1.305640  -2  6  4    2   72.3357  1.305641   -0.0001 -0.000001
   81.7642 1.177210   0  0 24    2   81.7609  1.177249   -0.0033 -0.000039

 rmse = 0.00003323556
 
     A =5.4670(8)              B =9.0668(7)               C =28.2947(6)          
 Alpha =90                  Beta =93.08(1)            Gamma =90                  
 
 Volume = 1400.5(1)