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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060816_Delhayelite_POWDER[1]
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.002
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   13.0347 6.785320   1  1  0    2   13.0423  6.781399    0.0076  0.003921
   28.3706 3.143031   7  1  0    2   28.3731  3.142755    0.0025  0.000277
   31.5248 2.835399   7  1  1    2   31.5272  2.835186    0.0024  0.000213
   30.1975 2.956926   1  1  2    2   30.1984  2.956836    0.0009  0.000090
   19.7653 4.487555   4  0  1    2   19.7657  4.487473    0.0004  0.000082
   25.2230 3.527632   0  2  0    2   25.2224  3.527709   -0.0006 -0.000077
   36.2531 2.475723   6  2  1    2   36.2515  2.475827   -0.0016 -0.000103
   25.6127 3.474839   6  0  1    2   25.6072  3.475570   -0.0055 -0.000731
    7.201512.261466   2  0  0    2    7.1872 12.285811   -0.0143 -0.024345

 rmse = 0.00002399163
 
     A =24.572(2)              B =7.0554(8)               C =6.5712(8)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 1139.2(2)