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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070374
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.058
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   16.9381 5.247973   0  2  0    2   16.9381  5.247971    0.0000  0.000002
   22.3941 3.976882   0  2  1    2   22.3914  3.977351   -0.0027 -0.000468
   25.0586 3.558750   1  1  1    2   25.0596  3.558608    0.0010  0.000142
   31.6245 2.831903   1  3  0    2   31.6227  2.832057   -0.0018 -0.000154
   34.9620 2.568382   1  3  1    2   34.9609  2.568460   -0.0011 -0.000077
   35.9101 2.502606   1  1  2    2   35.9116  2.502506    0.0015  0.000101
   51.3592 1.779416   2  2  2    2   51.3627  1.779304    0.0035  0.000112
   53.7832 1.704710   2  4  1    2   53.7803  1.704794   -0.0029 -0.000084
   54.5845 1.681537   0  6  1    2   54.5867  1.681473    0.0022  0.000063
   55.6787 1.651020   1  3  3    2   55.6759  1.651098   -0.0028 -0.000078
   56.5514 1.627568   1  5  2    2   56.5539  1.627501    0.0025  0.000067
   65.1500 1.431806   1  7  0    2   65.1488  1.431830   -0.0012 -0.000024

 rmse = 0.00002699197
 
     A =4.8233(3)              B =10.4959(2)              C =6.0966(3)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 308.64(2)