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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R040019FluororichteriteXrayPowderProfile
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.066
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   10.5292 8.447684   1  1  0    2   10.5299  8.447084    0.0007  0.000600
   18.2470 4.875350  -1  1  1    2   18.2490  4.874821    0.0020  0.000528
   19.7830 4.498879   0  4  0    2   19.7775  4.500122   -0.0055 -0.001243
   22.3033 3.994362   1  1  1    2   22.3202  3.991366    0.0169  0.002996
   23.0364 3.868514  -1  3  1    2   23.0277  3.869965   -0.0087 -0.001452
   26.4015 3.381339   1  3  1    2   26.4012  3.381376   -0.0003 -0.000037
   27.2534 3.277291   2  4  0    2   27.2519  3.277470   -0.0015 -0.000180
   28.4711 3.139504   3  1  0    2   28.4692  3.139705   -0.0019 -0.000202
   30.3837 2.945662   2  2  1    2   30.3718  2.946789   -0.0119 -0.001127
   31.8247 2.815218   3  3  0    2   31.8192  2.815695   -0.0055 -0.000476
   32.7648 2.736395  -3  3  1    2   32.7597  2.736812   -0.0051 -0.000416
   33.1725 2.703623   1  5  1    2   33.1767  2.703288    0.0042  0.000335
   34.7194 2.586394   0  6  1    2   34.7226  2.586165    0.0032  0.000229
   35.4846 2.532250  -2  0  2    2   35.4878  2.532030    0.0032  0.000220
   39.3256 2.292898  -1  7  1    2   39.3269  2.292826    0.0013  0.000072
   39.6280 2.276066  -3  1  2    2   39.6263  2.276160   -0.0017 -0.000094
   40.9322 2.206387  -2  4  2    2   40.9260  2.206706   -0.0062 -0.000319
   41.8058 2.162206   2  6  1    2   41.8081  2.162092    0.0023  0.000114
   44.2852 2.046551   2  0  2    2   44.2834  2.046630   -0.0018 -0.000080
   47.8303 1.902598   5  1  0    2   47.8346  1.902435    0.0043  0.000163
   55.5899 1.653674   4  6  1    2   55.5960  1.653508    0.0061  0.000166
   56.1463 1.638579   4  8  0    2   56.1405  1.638735   -0.0058 -0.000156
   57.1183 1.612950   1 11  0    2   57.1173  1.612976   -0.0010 -0.000027
   58.5908 1.575827  -1  5  3    2   58.5945  1.575736    0.0037  0.000091
   64.6301 1.442236  -6  6  1    2   64.6387  1.442065    0.0086  0.000171
   68.5369 1.369156   5  1  2    2   68.5327  1.369229   -0.0042 -0.000074
   73.3501 1.290654  -2 12  2    2   73.3559  1.290566    0.0058  0.000088
   80.1068 1.197835  -5 11  2    2   80.0990  1.197933   -0.0078 -0.000097

 rmse = 0.00005840655
 
     A =     9.8859(5)         B =    18.0004(8)          C =     5.2731(3)      
 Alpha =    90.             Beta =   104.623(5)       Gamma =    90.             
 
 Volume =    907.98(6)