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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060881_GartrelliteXrayPowderProfileCorrected
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.002
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   13.0223 6.791553   0  0  1    2   13.0185  6.793503   -0.0038 -0.001950
   19.2386 4.609104   1  0  1    2   19.2799  4.599316    0.0413  0.009788
   19.7690 4.486637   1  1  1    2   19.7556  4.489645   -0.0134 -0.003008
   21.8466 4.064476   1  1  0    2   21.8515  4.063581    0.0049  0.000895
   24.7994 3.586860  -1  0  1    2   24.7338  3.596229   -0.0656 -0.009370
   25.0286 3.554533   0 -1  1    2   25.0009  3.558404   -0.0277 -0.003871
   30.2261 2.954157  -1 -1  1    2   30.2608  2.950847    0.0347  0.003310
   30.8114 2.899365  -1  1  1    2   30.8478  2.896030    0.0364  0.003334
   32.4307 2.758208   1  2  1    2   32.4223  2.758901   -0.0084 -0.000693
   33.0872 2.704970   2  1  1    2   33.0896  2.704777    0.0024  0.000193
   44.5205 2.033296  -2  1  0    2   44.5136  2.033597   -0.0069 -0.000301
   64.0664 1.452186  -2  1  3    2   64.0661  1.452192   -0.0003 -0.000005

 rmse = 0.00025492554
 
     A =5.472(5)               B =5.613(6)                C =7.61(2)             
 Alpha =67.3(1)             Beta =69.3(1)             Gamma =69.57(6)            
 
 Volume = 195.5(4)