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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 R050439_Germanite_POWDER[1]
 
 Symmetry constraint is: CUBIC       
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.073
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   11.8348 7.517570   1  1  0    2   11.8575  7.503135    0.0227  0.014435
   20.5402 4.335581   2  1  1    2   20.5576  4.331937    0.0174  0.003644
   29.2273 3.060478   2  2  2    2   29.2014  3.063142   -0.0259 -0.002664
   31.5784 2.837247   3  2  1    2   31.5935  2.835919    0.0151  0.001329
   33.8124 2.654318   4  0  0    2   33.8328  2.652759    0.0204  0.001559
   48.5852 1.874990   4  4  0    2   48.5633  1.875784   -0.0219 -0.000794
   57.6401 1.599737   6  2  2    2   57.6426  1.599674    0.0025  0.000063
   78.5902 1.217212   6  6  2    2   78.5935  1.217169    0.0033  0.000043

 rmse = 0.00014624777
 
     A =10.6110(9)             B =10.6110(9)              C =10.6110(9)          
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 1194.7(3)