******************************************************************************
       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 R060268_02
 
 Symmetry constraint is: HEXAGONAL   
 
 Wavelength #1 =  0.710710
 Wavelength #2 =  0.709270
 Wavelength #3 =  0.713590
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.025
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.2009 4.409357   1  2  0    2    9.2062  4.406843    0.0053  0.002514
   10.4442 3.886941   3  0  0    2   10.4455  3.886470    0.0013  0.000470
   11.4897 3.535063   1  2  1    2   11.4942  3.533695    0.0045  0.001368
   12.0923 3.359876   2  2  0    2   12.0710  3.365782   -0.0213 -0.005906
   12.5741 3.231884   3  1  0    2   12.5668  3.233739   -0.0073 -0.001854
   16.0005 2.544064   4  1  0    2   15.9991  2.544292   -0.0014 -0.000228
   16.5955 2.453597   1  2  2    2   16.5827  2.455473   -0.0128 -0.001877
   21.2867 1.917848   4  3  0    2   21.2985  1.916795    0.0118  0.001053
   25.9097 1.580375   5  2  2    2   25.9381  1.578674    0.0284  0.001701
   28.8251 1.423569   7  2  0    2   28.8074  1.424424   -0.0177 -0.000855
   32.1914 1.278168   4  1  4    2   32.1867  1.278349   -0.0047 -0.000181
   33.6203 1.225357   5  5  2    2   33.6221  1.225294    0.0018  0.000063

 rmse = 0.00037429475
 
     A =13.463(3)              B =13.463(3)               C =5.914(2)            
 Alpha =90                  Beta =90                  Gamma =120                 
 
 Volume = 928.3(4)