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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060062
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.026
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.6948 9.139710   0  2  0    2    9.7000  9.134846    0.0052  0.004864
   10.6320 8.334111   1  1  0    2   10.6410  8.327058    0.0090  0.007052
   18.9891 4.675955   2  0  0    2   18.9822  4.677651   -0.0069 -0.001697
   19.4417 4.567964   0  4  0    2   19.4440  4.567423    0.0023  0.000541
   21.3460 4.164065   2  2  0    2   21.3488  4.163529    0.0028  0.000536
   27.2957 3.267564   2  4  0    2   27.2926  3.267930   -0.0031 -0.000367
   29.0490 3.074034   3  1  0    2   29.0496  3.073976    0.0006  0.000058
   32.2487 2.775715   3  3  0    2   32.2490  2.775686    0.0003  0.000029
   32.5080 2.754146   1  5  1    2   32.5081  2.754139    0.0001  0.000008
   34.1126 2.628079   0  6  1    2   34.1086  2.628381   -0.0040 -0.000302
   41.1220 2.194569   2  6  1    2   41.1266  2.194335    0.0046  0.000234
   55.2482 1.661987   4  6  1    2   55.2469  1.662024   -0.0013 -0.000037
   66.3570 1.408034  -6  6  1    2   66.3573  1.408028    0.0003  0.000006

 rmse = 0.00002587281
 
     A =9.5681(4)              B =18.270(3)               C =5.324(3)            
 Alpha =90                  Beta =102.107(8)          Gamma =90                  
 
 Volume = 910.0(3)