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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060900
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.009
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   15.3894 5.756203   0  1  0    2   15.3885  5.756535   -0.0009 -0.000333
   18.3860 4.823786   1  0  0    2   18.3877  4.823336    0.0017  0.000450
   23.5752 3.772038   0  1  1    2   23.5764  3.771847    0.0012  0.000191
   24.0587 3.697288   1  1  0    2   24.0600  3.697093    0.0013  0.000195
   29.8437 2.992239   1  1  1    2   29.8465  2.991967    0.0028  0.000272
   30.2693 2.951117  -1  1  1    2   30.2715  2.950911    0.0022  0.000206
   31.0612 2.877639   0  2  0    2   31.0542  2.878268   -0.0070 -0.000629
   37.2742 2.410900   2  0  0    2   37.2619  2.411668   -0.0123 -0.000768
   40.8686 2.206728  -1  2  1    2   40.8703  2.206641    0.0017  0.000087
   44.8684 2.018819  -2  1  1    2   44.8678  2.018843   -0.0006 -0.000024
   47.3398 1.919007   0  3  0    2   47.3440  1.918845    0.0042  0.000162
   48.2228 1.885904   0  2  2    2   48.2223  1.885924   -0.0005 -0.000019
   49.2518 1.848876   2  2  0    2   49.2612  1.848547    0.0094  0.000330
   51.2038 1.782870   1  3  0    2   51.2017  1.782937   -0.0021 -0.000067
   67.7123 1.382798   0  4  1    2   67.7101  1.382838   -0.0022 -0.000040

 rmse = 0.00005262850
 
     A =4.8242(5)              B =5.7565(3)               C =4.9939(8)           
 Alpha =90                  Beta =88.92(2)            Gamma =90                  
 
 Volume = 138.66(2)