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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R090030
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.016
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   19.3454 4.580812   0  2  0    2   19.3514  4.579403    0.0060  0.001409
   20.8321 4.257379  -1  2  1    2   20.8368  4.256436    0.0047  0.000943
   22.2086 3.996703  -1  2  0    2   22.1984  3.998515   -0.0102 -0.001812
   22.8417 3.887414  -1 -2  1    2   22.8480  3.886358    0.0063  0.001056
   27.7498 3.210376  -2  1  0    2   27.7483  3.210542   -0.0015 -0.000166
   29.8662 2.987641  -1  3  1    2   29.8685  2.987415    0.0023  0.000226
   32.7790 2.728627  -1  0  4    2   32.7791  2.728621    0.0001  0.000006
   34.0295 2.631209  -1 -1  4    2   34.0271  2.631390   -0.0024 -0.000181
   37.5701 2.391082  -1 -3  3    2   37.5678  2.391224   -0.0023 -0.000142
   38.5635 2.331767   1  3  1    2   38.5612  2.331903   -0.0023 -0.000136
   44.2066 2.046423   0 -2  4    2   44.2092  2.046311    0.0026  0.000112
   51.3355 1.777813  -4 -2  2    2   51.3359  1.777799    0.0004  0.000014

 rmse = 0.00003730800
 
     A =8.861(2)               B =9.2396(9)               C =11.952(2)           
 Alpha =88.14(1)            Beta =131.95(1)           Gamma =96.70(1)            
 
 Volume = 721.3(1)