Jamesonite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern for R050430 Niizeki N, Buerger M J Zeitschrift fur Kristallographie 109 (1957) 161-183 The crystal structure of jamesonite, FePb4Sb6S14 CELL PARAMETERS: 15.57000 18.98000 4.030000 90.00000 91.80000 90.00000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 2-THETA INTENSITY D-SPACING H K L 9.28 7.37 9.4840 0 2 0 10.86 16.33 8.1100 1 2 0 11.26 1.16 7.8218 2 0 0 14.63 8.98 6.0343 2 2 0 15.06 3.67 5.8620 1 3 0 17.59 7.72 5.0280 3 1 0 19.51 1.79 4.5381 1 4 0 21.86 30.13 4.0550 2 4 0 22.10 7.42 4.0127 0 0 1 22.04 2.70 4.0229 3 3 0 22.68 15.11 3.9109 4 0 0 23.16 40.15 3.8303 4 1 0 23.47 9.26 3.7804 1 1 1 24.02 28.12 3.6955 0 2 1 24.08 2.83 3.6868 1 5 0 24.53 4.51 3.6200 -1 2 1 24.86 36.43 3.5735 1 2 1 25.00 1.24 3.5527 -2 1 1 25.20 2.25 3.5256 2 0 1 25.33 7.74 3.5083 3 4 0 25.64 2.54 3.4662 2 1 1 26.05 100.00 3.4133 2 5 0 26.24 1.54 3.3880 0 3 1 26.31 3.46 3.3793 -2 2 1 26.71 13.01 3.3295 -1 3 1 26.74 5.78 3.3260 4 3 0 26.92 5.60 3.3046 2 2 1 27.01 1.05 3.2932 1 3 1 27.96 3.68 3.1837 -3 1 1 28.37 43.64 3.1394 -2 3 1 28.75 2.63 3.0987 1 6 0 28.93 13.08 3.0792 2 3 1 28.86 16.79 3.0870 5 1 0 29.05 14.43 3.0677 3 5 0 29.15 2.74 3.0571 -3 2 1 29.52 3.33 3.0198 -1 4 1 29.97 16.56 2.9748 3 2 1 30.43 12.32 2.9310 2 6 0 31.03 1.52 2.8758 -2 4 1 31.03 11.60 2.8761 -3 3 1 31.37 3.29 2.8458 -4 0 1 31.56 4.69 2.8293 2 4 1 31.73 53.74 2.8143 -4 1 1 31.81 43.35 2.8072 3 3 1 31.85 1.68 2.8042 5 3 0 32.41 1.25 2.7567 0 5 1 32.40 5.04 2.7577 4 0 1 32.75 24.41 2.7290 4 1 1 32.79 22.68 2.7257 -4 2 1 32.82 1.62 2.7230 4 5 0 33.07 25.61 2.7033 3 6 0 33.50 1.55 2.6700 1 7 0 33.51 7.96 2.6693 -3 4 1 34.19 1.53 2.6177 -2 5 1 34.24 11.25 2.6139 3 4 1 34.67 2.60 2.5825 2 5 1 34.98 2.18 2.5604 2 7 0 35.44 1.86 2.5278 4 3 1 35.65 3.86 2.5140 6 2 0 36.46 3.93 2.4600 -1 6 1 36.47 1.06 2.4591 -3 5 1 36.68 2.06 2.4452 1 6 1 37.04 5.44 2.4227 -5 2 1 37.72 4.72 2.3802 -2 6 1 37.88 1.35 2.3710 0 8 0 38.17 6.74 2.3537 2 6 1 38.15 5.81 2.3545 5 2 1 38.33 2.05 2.3442 1 8 0 39.37 18.54 2.2847 6 4 0 39.65 1.61 2.2691 2 8 0 39.66 8.31 2.2687 5 3 1 40.08 3.16 2.2456 0 7 1 40.41 19.33 2.2284 -1 7 1 40.43 4.82 2.2273 4 7 0 40.49 3.17 2.2238 5 6 0 40.89 1.58 2.2034 -6 1 1 41.57 6.42 2.1686 -2 7 1 41.44 1.69 2.1752 7 2 0 41.78 1.95 2.1584 3 8 0 41.74 1.17 2.1601 -6 2 1 41.98 1.22 2.1485 2 7 1 42.68 1.49 2.1151 -4 6 1 42.85 1.76 2.1071 7 3 0 42.96 7.18 2.1020 6 2 1 43.47 1.76 2.0782 4 6 1 43.52 5.03 2.0758 -3 7 1 44.11 6.14 2.0495 3 7 1 44.30 24.21 2.0413 0 8 1 44.32 9.18 2.0403 6 3 1 44.79 6.29 2.0200 1 8 1 45.11 12.98 2.0063 0 0 2 44.76 13.10 2.0216 7 4 0 44.99 6.25 2.0114 6 6 0 45.04 10.09 2.0094 -6 4 1 45.38 10.41 1.9952 0 1 2 45.58 6.09 1.9870 -1 1 2 46.37 6.65 1.9551 -1 2 2 46.15 1.32 1.9637 -5 6 1 46.36 3.15 1.9555 8 0 0 46.62 2.61 1.9451 8 1 0 46.93 6.72 1.9328 4 7 1 46.82 2.78 1.9373 -7 2 1 47.12 2.03 1.9255 7 5 0 47.40 6.13 1.9150 -6 5 1 47.39 1.96 1.9152 8 2 0 47.88 9.11 1.8968 0 10 0 48.05 2.87 1.8906 3 8 1 48.25 4.96 1.8830 1 10 0 48.11 6.16 1.8883 7 2 1 48.59 1.05 1.8706 -2 3 2 48.50 3.54 1.8741 6 5 1 49.00 1.16 1.8560 -3 2 2 49.02 7.50 1.8553 4 9 0 49.18 3.39 1.8496 1 9 1 49.33 1.43 1.8443 3 1 2 49.78 1.76 1.8288 1 4 2 49.99 5.71 1.8216 -4 8 1 49.85 4.65 1.8264 -7 4 1 49.90 8.50 1.8249 7 6 0 50.24 3.38 1.8131 -3 3 2 50.16 10.23 1.8159 -6 6 1 50.38 3.82 1.8084 -4 0 2 50.35 6.10 1.8094 5 7 1 51.04 10.38 1.7867 2 4 2 51.17 1.08 1.7825 3 10 0 51.24 2.96 1.7800 -8 0 1 51.78 2.42 1.7628 4 0 2 51.49 3.68 1.7722 -8 1 1 52.02 6.68 1.7552 4 1 2 52.04 2.59 1.7546 -7 5 1 52.25 2.32 1.7480 5 9 0 52.51 11.39 1.7401 -2 5 2 52.21 1.04 1.7495 -8 2 1 52.81 4.01 1.7309 9 1 0 53.24 2.36 1.7180 7 5 1 53.62 6.56 1.7067 4 10 0 53.57 4.43 1.7081 8 2 1 53.52 2.43 1.7097 9 2 0 54.07 1.78 1.6935 -3 5 2 53.94 1.78 1.6972 5 8 1 54.07 4.08 1.6937 -4 9 1 54.32 1.61 1.6863 -5 2 2 54.30 1.88 1.6869 6 7 1 54.56 2.84 1.6794 1 6 2 54.73 3.02 1.6745 4 9 1 55.15 1.90 1.6630 8 6 0 55.48 1.51 1.6539 -5 3 2 55.74 5.34 1.6466 2 6 2 56.09 1.72 1.6372 3 11 0 56.29 2.00 1.6320 9 4 0 57.01 1.17 1.6129 -5 9 1 57.52 1.52 1.5998 1 7 2 57.57 4.55 1.5987 3 6 2 57.84 2.60 1.5919 -6 2 2 58.03 1.12 1.5872 -2 7 2 58.74 1.46 1.5697 -4 6 2 58.96 1.46 1.5644 10 0 0 59.49 2.50 1.5516 -3 7 2 59.18 2.00 1.5591 10 1 0 59.83 1.58 1.5435 10 2 0 60.35 1.99 1.5316 0 8 2 60.51 1.01 1.5278 -1 8 2 60.28 1.17 1.5333 7 9 0 60.48 1.76 1.5286 -6 4 2 60.81 2.21 1.5211 -3 11 1 61.30 4.47 1.5102 5 11 0 61.57 3.20 1.5042 -4 7 2 61.37 1.40 1.5086 8 8 0 61.86 1.37 1.4978 -7 2 2 62.34 2.64 1.4874 6 4 2 62.42 2.17 1.4858 -6 5 2 62.94 2.42 1.4748 -4 11 1 63.36 1.47 1.4658 -1 12 1 63.52 3.39 1.4627 1 12 1 63.55 1.22 1.4621 4 11 1 63.55 1.19 1.4620 8 7 1 63.98 2.76 1.4532 0 9 2 64.24 7.37 1.4479 6 5 2 64.40 1.09 1.4447 -7 4 2 64.52 3.66 1.4423 2 12 1 64.33 1.99 1.4462 10 5 0 65.04 1.48 1.4320 7 3 2 64.97 1.13 1.4335 8 9 0 64.90 1.88 1.4348 -10 3 1 65.63 1.07 1.4205 -5 11 1 65.76 1.62 1.4182 11 1 0 66.53 2.83 1.4036 6 6 2 66.39 2.84 1.4061 10 3 1 66.67 3.57 1.4009 8 8 1 66.62 1.08 1.4018 9 8 0 67.33 1.27 1.3888 -5 8 2 67.37 2.23 1.3882 -8 3 2 67.47 1.20 1.3864 -9 7 1 67.91 1.10 1.3783 0 10 2 67.88 3.34 1.3789 8 0 2 67.83 1.36 1.3799 10 4 1 68.19 4.23 1.3733 -10 5 1 68.52 2.08 1.3676 -7 6 2 68.79 1.02 1.3630 9 7 1 68.87 1.63 1.3615 8 10 0 68.96 1.12 1.3599 -8 9 1 69.36 5.48 1.3531 -2 13 1 69.41 3.23 1.3522 4 9 2 69.65 1.45 1.3482 2 13 1 69.65 1.56 1.3481 10 5 1 70.28 1.86 1.3376 0 0 3 70.15 1.08 1.3397 -3 10 2 70.44 2.06 1.3350 2 14 0 70.66 2.26 1.3314 -9 1 2 71.21 1.12 1.3224 5 13 0 72.06 3.44 1.3089 -4 10 2 71.85 1.65 1.3122 10 6 1 73.07 1.05 1.2933 -3 2 3 72.76 2.14 1.2980 -8 10 1 73.83 1.04 1.2819 9 2 2 73.90 1.23 1.2808 8 10 1 74.29 1.36 1.2751 -4 1 3 73.88 1.31 1.2812 -9 9 1 74.34 2.23 1.2743 3 2 3 74.11 1.04 1.2777 -7 8 2 74.32 1.66 1.2747 6 12 1 74.88 2.74 1.2665 -4 2 3 74.42 1.50 1.2732 10 7 1 75.04 1.32 1.2641 2 4 3 75.17 2.35 1.2624 3 11 2 75.32 1.27 1.2601 3 3 3 75.30 1.31 1.2604 1 15 0 75.35 2.26 1.2598 -8 7 2 75.96 2.27 1.2512 -2 5 3 76.09 1.04 1.2494 -3 14 1 76.16 2.00 1.2483 2 15 0 76.56 1.33 1.2428 4 2 3 75.94 1.36 1.2515 -12 0 1 76.80 1.48 1.2396 2 5 3 76.79 1.33 1.2396 -1 12 2 76.88 1.07 1.2385 -8 11 1 76.72 1.08 1.2407 -12 2 1 77.34 1.07 1.2322 10 8 1 78.11 1.06 1.2221 7 12 1 77.81 3.14 1.2260 12 1 1 78.95 1.54 1.2111 -11 7 1 79.40 1.90 1.2054 10 2 2 79.95 1.94 1.1985 -1 7 3 79.65 2.23 1.2022 6 14 0 81.11 1.08 1.1842 -6 3 3 81.52 1.12 1.1793 -8 9 2 82.45 1.77 1.1684 -6 4 3 83.23 1.23 1.1594 1 8 3 82.90 1.63 1.1632 7 13 1 83.58 2.71 1.1554 6 3 3 83.41 1.20 1.1574 10 5 2 84.69 1.10 1.1431 -11 4 2 86.25 1.74 1.1264 -6 6 3 85.99 1.00 1.1292 -9 12 1 87.00 1.61 1.1186 -8 1 3 87.06 1.87 1.1180 -7 14 1 87.32 2.96 1.1153 8 10 2 87.76 1.13 1.1109 -5 13 2 88.02 1.67 1.1082 4 8 3 87.98 2.09 1.1087 2 14 2 88.17 1.06 1.1068 -12 8 1 88.17 1.06 1.1068 -12 8 1 XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.