Jamesonite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern for R050431 Niizeki N, Buerger M J Zeitschrift fur Kristallographie 109 (1957) 161-183 The crystal structure of jamesonite, FePb4Sb6S14 CELL PARAMETERS: 15.77546 19.10311 4.007534 90.00000 91.58108 90.00000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 2-THETA INTENSITY D-SPACING H K L 9.27 7.37 9.5516 0 2 0 10.84 16.33 8.1698 1 2 0 11.23 1.16 7.8847 2 0 0 14.57 8.98 6.0806 2 2 0 15.01 3.67 5.9045 1 3 0 17.50 7.72 5.0681 3 1 0 19.42 1.79 4.5708 1 4 0 21.75 30.13 4.0849 2 4 0 22.19 7.42 4.0060 0 0 1 21.92 2.70 4.0537 3 3 0 22.55 15.11 3.9424 4 0 0 23.03 40.15 3.8610 4 1 0 23.53 9.26 3.7811 1 1 1 24.09 28.12 3.6942 0 2 1 23.96 2.83 3.7132 1 5 0 24.61 4.51 3.6174 -1 2 1 24.89 36.43 3.5767 1 2 1 25.09 1.24 3.5491 -2 1 1 25.21 2.25 3.5323 2 0 1 25.19 7.74 3.5347 3 4 0 25.64 2.54 3.4735 2 1 1 25.91 100.00 3.4382 2 5 0 26.28 1.54 3.3908 0 3 1 26.37 3.46 3.3785 -2 2 1 26.76 13.01 3.3311 -1 3 1 26.59 5.78 3.3519 4 3 0 26.90 5.60 3.3130 2 2 1 27.02 1.05 3.2992 1 3 1 28.01 3.68 3.1843 -3 1 1 28.40 43.64 3.1417 -2 3 1 28.59 2.63 3.1209 1 6 0 28.90 13.08 3.0889 2 3 1 28.68 16.79 3.1118 5 1 0 28.88 14.43 3.0905 3 5 0 29.18 2.74 3.0593 -3 2 1 29.52 3.33 3.0247 -1 4 1 29.91 16.56 2.9869 3 2 1 30.26 12.32 2.9522 2 6 0 31.03 1.52 2.8808 -2 4 1 31.04 11.60 2.8802 -3 3 1 31.38 3.29 2.8495 -4 0 1 31.49 4.69 2.8399 2 4 1 31.74 53.74 2.8183 -4 1 1 31.72 43.35 2.8196 3 3 1 31.65 1.68 2.8262 5 3 0 32.37 1.25 2.7648 0 5 1 32.28 5.04 2.7719 4 0 1 32.63 24.41 2.7432 4 1 1 32.79 22.68 2.7306 -4 2 1 32.63 1.62 2.7436 4 5 0 32.88 25.61 2.7233 3 6 0 33.31 1.55 2.6890 1 7 0 33.48 7.96 2.6752 -3 4 1 34.15 1.53 2.6247 -2 5 1 34.13 11.25 2.6264 3 4 1 34.57 2.60 2.5937 2 5 1 34.77 2.18 2.5789 2 7 0 35.30 1.86 2.5416 4 3 1 35.41 3.86 2.5341 6 2 0 36.38 3.93 2.4685 -1 6 1 36.41 1.06 2.4664 -3 5 1 36.58 2.06 2.4555 1 6 1 36.99 5.44 2.4294 -5 2 1 37.65 4.72 2.3884 -2 6 1 37.65 1.35 2.3879 0 8 0 38.03 6.74 2.3650 2 6 1 37.96 5.81 2.3691 5 2 1 38.10 2.05 2.3610 1 8 0 39.10 18.54 2.3026 6 4 0 39.41 1.61 2.2854 2 8 0 39.45 8.31 2.2829 5 3 1 39.96 3.16 2.2554 0 7 1 40.29 19.33 2.2376 -1 7 1 40.17 4.82 2.2439 4 7 0 40.23 3.17 2.2407 5 6 0 40.80 1.58 2.2109 -6 1 1 41.45 6.42 2.1774 -2 7 1 41.15 1.69 2.1926 7 2 0 41.52 1.95 2.1741 3 8 0 41.64 1.17 2.1678 -6 2 1 41.81 1.22 2.1596 2 7 1 42.56 1.49 2.1233 -4 6 1 42.55 1.76 2.1238 7 3 0 42.71 7.18 2.1163 6 2 1 43.26 1.76 2.0906 4 6 1 43.39 5.03 2.0844 -3 7 1 43.91 6.14 2.0611 3 7 1 44.13 24.21 2.0511 0 8 1 44.06 9.18 2.0542 6 3 1 44.61 6.29 2.0303 1 8 1 45.25 12.98 2.0030 0 0 2 44.44 13.10 2.0375 7 4 0 44.69 6.25 2.0269 6 6 0 44.91 10.09 2.0175 -6 4 1 45.51 10.41 1.9921 0 1 2 45.73 6.09 1.9832 -1 1 2 46.50 6.65 1.9519 -1 2 2 46.00 1.32 1.9721 -5 6 1 46.02 3.15 1.9712 8 0 0 46.28 2.61 1.9608 8 1 0 46.68 6.72 1.9447 4 7 1 46.66 2.78 1.9455 -7 2 1 46.79 2.03 1.9406 7 5 0 47.24 6.13 1.9233 -6 5 1 47.05 1.96 1.9305 8 2 0 47.58 9.11 1.9103 0 10 0 47.80 2.87 1.9017 3 8 1 47.95 4.96 1.8964 1 10 0 47.80 6.16 1.9020 7 2 1 48.72 1.05 1.8682 -2 3 2 48.20 3.54 1.8870 6 5 1 49.14 1.16 1.8532 -3 2 2 48.70 7.50 1.8689 4 9 0 48.96 3.39 1.8596 1 9 1 49.34 1.43 1.8461 3 1 2 49.82 1.76 1.8292 1 4 2 49.80 5.71 1.8302 -4 8 1 49.67 4.65 1.8347 -7 4 1 49.54 8.50 1.8390 7 6 0 50.36 3.38 1.8111 -3 3 2 49.97 10.23 1.8243 -6 6 1 50.51 3.82 1.8060 -4 0 2 50.06 6.10 1.8212 5 7 1 51.04 10.38 1.7884 2 4 2 50.83 1.08 1.7954 3 10 0 51.04 2.96 1.7883 -8 0 1 51.73 2.42 1.7662 4 0 2 51.28 3.68 1.7805 -8 1 1 51.97 6.68 1.7587 4 1 2 51.83 2.59 1.7630 -7 5 1 51.90 2.32 1.7609 5 9 0 52.57 11.39 1.7399 -2 5 2 52.00 1.04 1.7578 -8 2 1 52.41 4.01 1.7448 9 1 0 52.88 2.36 1.7304 7 5 1 53.26 6.56 1.7191 4 10 0 53.19 4.43 1.7210 8 2 1 53.11 2.43 1.7234 9 2 0 54.13 1.78 1.6934 -3 5 2 53.61 1.78 1.7085 5 8 1 53.83 4.08 1.7022 -4 9 1 54.40 1.61 1.6855 -5 2 2 53.95 1.88 1.6986 6 7 1 54.54 2.84 1.6815 1 6 2 54.41 3.02 1.6852 4 9 1 54.74 1.90 1.6760 8 6 0 55.54 1.51 1.6536 -5 3 2 55.69 5.34 1.6496 2 6 2 55.71 1.72 1.6490 3 11 0 55.86 2.00 1.6449 9 4 0 56.75 1.17 1.6213 -5 9 1 57.47 1.52 1.6027 1 7 2 57.47 4.55 1.6027 3 6 2 57.88 2.60 1.5921 -6 2 2 58.01 1.12 1.5889 -2 7 2 58.74 1.46 1.5709 -4 6 2 58.50 1.46 1.5769 10 0 0 59.47 2.50 1.5533 -3 7 2 58.71 2.00 1.5716 10 1 0 59.37 1.58 1.5559 10 2 0 60.27 1.99 1.5346 0 8 2 60.45 1.01 1.5305 -1 8 2 59.83 1.17 1.5449 7 9 0 60.49 1.76 1.5297 -6 4 2 60.49 2.21 1.5295 -3 11 1 60.86 4.47 1.5213 5 11 0 61.54 3.20 1.5061 -4 7 2 60.91 1.40 1.5202 8 8 0 61.86 1.37 1.4990 -7 2 2 62.11 2.64 1.4935 6 4 2 62.40 2.17 1.4873 -6 5 2 62.60 2.42 1.4829 -4 11 1 63.01 1.47 1.4743 -1 12 1 63.14 3.39 1.4715 1 12 1 63.14 1.22 1.4717 4 11 1 63.08 1.19 1.4729 8 7 1 63.86 2.76 1.4568 0 9 2 64.00 7.37 1.4540 6 5 2 64.37 1.09 1.4465 -7 4 2 64.13 3.66 1.4513 2 12 1 63.82 1.99 1.4577 10 5 0 64.76 1.48 1.4386 7 3 2 64.47 1.13 1.4444 8 9 0 64.55 1.88 1.4428 -10 3 1 65.28 1.07 1.4285 -5 11 1 65.22 1.62 1.4296 11 1 0 66.25 2.83 1.4098 6 6 2 65.86 2.84 1.4173 10 3 1 66.17 3.57 1.4113 8 8 1 66.10 1.08 1.4127 9 8 0 67.24 1.27 1.3915 -5 8 2 67.30 2.23 1.3904 -8 3 2 67.09 1.20 1.3942 -9 7 1 67.74 1.10 1.3824 0 10 2 67.54 3.34 1.3860 8 0 2 67.28 1.36 1.3907 10 4 1 67.81 4.23 1.3812 -10 5 1 68.43 2.08 1.3701 -7 6 2 68.25 1.02 1.3734 9 7 1 68.34 1.63 1.3718 8 10 0 68.57 1.12 1.3676 -8 9 1 68.95 5.48 1.3611 -2 13 1 69.15 3.23 1.3576 4 9 2 69.20 1.45 1.3568 2 13 1 69.09 1.56 1.3587 10 5 1 70.47 1.86 1.3353 0 0 3 70.00 1.08 1.3432 -3 10 2 69.92 2.06 1.3445 2 14 0 70.56 2.26 1.3339 -9 1 2 70.68 1.12 1.3320 5 13 0 71.90 3.44 1.3124 -4 10 2 71.27 1.65 1.3224 10 6 1 73.29 1.05 1.2909 -3 2 3 72.33 2.14 1.3055 -8 10 1 73.40 1.04 1.2892 9 2 2 73.33 1.23 1.2903 8 10 1 74.51 1.36 1.2727 -4 1 3 73.43 1.31 1.2887 -9 9 1 74.40 2.23 1.2743 3 2 3 73.95 1.04 1.2810 -7 8 2 73.77 1.66 1.2836 6 12 1 75.09 2.74 1.2643 -4 2 3 73.81 1.50 1.2831 10 7 1 75.11 1.32 1.2639 2 4 3 74.85 2.35 1.2677 3 11 2 75.36 1.27 1.2604 3 3 3 74.73 1.31 1.2694 1 15 0 75.18 2.26 1.2630 -8 7 2 76.11 2.27 1.2498 -2 5 3 75.61 1.04 1.2569 -3 14 1 75.58 2.00 1.2572 2 15 0 76.56 1.33 1.2436 4 2 3 75.46 1.36 1.2590 -12 0 1 76.84 1.48 1.2397 2 5 3 76.53 1.33 1.2441 -1 12 2 76.40 1.07 1.2459 -8 11 1 76.23 1.08 1.2482 -12 2 1 76.70 1.07 1.2417 10 8 1 77.50 1.06 1.2309 7 12 1 77.12 3.14 1.2360 12 1 1 78.44 1.54 1.2185 -11 7 1 78.87 1.90 1.2128 10 2 2 80.02 1.94 1.1982 -1 7 3 79.01 2.23 1.2110 6 14 0 81.27 1.08 1.1830 -6 3 3 81.27 1.12 1.1830 -8 9 2 82.58 1.77 1.1675 -6 4 3 83.21 1.23 1.1603 1 8 3 82.23 1.63 1.1716 7 13 1 83.42 2.71 1.1578 6 3 3 82.84 1.20 1.1646 10 5 2 84.42 1.10 1.1467 -11 4 2 86.33 1.74 1.1262 -6 6 3 85.39 1.00 1.1361 -9 12 1 87.11 1.61 1.1181 -8 1 3 86.45 1.87 1.1249 -7 14 1 86.75 2.96 1.1218 8 10 2 87.39 1.13 1.1151 -5 13 2 87.86 1.67 1.1104 4 8 3 87.51 2.09 1.1139 2 14 2 87.54 1.06 1.1137 -12 8 1 87.54 1.06 1.1137 -12 8 1 XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.