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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050481
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.031
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   10.8701 8.155492   1  2  0    2   10.8646  8.159639   -0.0055 -0.004147
   14.6322 6.061561   2  2  0    2   14.6262  6.064022   -0.0060 -0.002461
   17.5859 5.047772   3  1  0    2   17.5900  5.046609    0.0041  0.001163
   21.7960 4.079946   2  4  0    2   21.7967  4.079819    0.0007  0.000127
   22.6724 3.923964   4  0  0    2   22.6700  3.924377   -0.0024 -0.000413
   23.1462 3.844594   4  1  0    2   23.1492  3.844099    0.0030  0.000496
   24.8288 3.587409   1  2  1    2   24.8329  3.586828    0.0041  0.000581
   25.9456 3.435286   2  5  0    2   25.9463  3.435201    0.0007  0.000085
   28.3201 3.152105  -2  3  1    2   28.3187  3.152262   -0.0014 -0.000158
   29.9339 2.985565   3  2  1    2   29.9318  2.985766   -0.0021 -0.000201

 rmse = 0.00002055678
 
     A =    15.705(2)          B =    19.102(2)           C =     4.0271(4)      
 Alpha =    90.             Beta =    91.79(1)        Gamma =    90.             
 
 Volume =   1207.6(2)