Jamesonite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern for R050481 Niizeki N, Buerger M J Zeitschrift fur Kristallographie 109 (1957) 161-183 The crystal structure of jamesonite, FePb4Sb6S14 CELL PARAMETERS: 15.70518 19.10285 4.027189 90.00000 91.79127 90.00000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 2-THETA INTENSITY D-SPACING H K L 9.28 7.37 9.5514 0 2 0 10.86 16.33 8.1596 1 2 0 11.30 1.16 7.8488 2 0 0 14.63 8.98 6.0640 2 2 0 15.03 3.67 5.9006 1 3 0 17.59 7.72 5.0466 3 1 0 19.44 1.79 4.5689 1 4 0 21.80 30.13 4.0798 2 4 0 22.10 7.42 4.0252 0 0 1 22.00 2.70 4.0427 3 3 0 22.67 15.11 3.9244 4 0 0 23.15 40.15 3.8441 4 1 0 23.46 9.26 3.7930 1 1 1 24.00 28.12 3.7093 0 2 1 23.98 2.83 3.7122 1 5 0 24.51 4.51 3.6334 -1 2 1 24.83 36.43 3.5868 1 2 1 24.99 1.24 3.5643 -2 1 1 25.19 2.25 3.5371 2 0 1 25.26 7.74 3.5274 3 4 0 25.62 2.54 3.4779 2 1 1 25.95 100.00 3.4352 2 5 0 26.20 1.54 3.4024 0 3 1 26.29 3.46 3.3916 -2 2 1 26.67 13.01 3.3435 -1 3 1 26.69 5.78 3.3409 4 3 0 26.89 5.60 3.3169 2 2 1 26.97 1.05 3.3072 1 3 1 27.94 3.68 3.1941 -3 1 1 28.32 43.64 3.1523 -2 3 1 28.61 2.63 3.1203 1 6 0 28.88 13.08 3.0920 2 3 1 28.83 16.79 3.0979 5 1 0 28.94 14.43 3.0856 3 5 0 29.11 2.74 3.0681 -3 2 1 29.45 3.33 3.0340 -1 4 1 29.93 16.56 2.9858 3 2 1 30.30 12.32 2.9503 2 6 0 30.96 1.52 2.8889 -2 4 1 30.97 11.60 2.8875 -3 3 1 31.34 3.29 2.8549 -4 0 1 31.48 4.69 2.8424 2 4 1 31.69 53.74 2.8235 -4 1 1 31.75 43.35 2.8186 3 3 1 31.78 1.68 2.8158 5 3 0 32.31 1.25 2.7711 0 5 1 32.36 5.04 2.7670 4 0 1 32.70 24.41 2.7385 4 1 1 32.74 22.68 2.7353 -4 2 1 32.72 1.62 2.7375 4 5 0 32.93 25.61 2.7199 3 6 0 33.33 1.55 2.6887 1 7 0 33.42 7.96 2.6810 -3 4 1 34.08 1.53 2.6308 -2 5 1 34.15 11.25 2.6256 3 4 1 34.56 2.60 2.5955 2 5 1 34.81 2.18 2.5776 2 7 0 35.37 1.86 2.5378 4 3 1 35.58 3.86 2.5233 6 2 0 36.32 3.93 2.4735 -1 6 1 36.36 1.06 2.4710 -3 5 1 36.55 2.06 2.4587 1 6 1 36.97 5.44 2.4312 -5 2 1 37.58 4.72 2.3930 -2 6 1 37.67 1.35 2.3879 0 8 0 38.02 6.74 2.3664 2 6 1 38.08 5.81 2.3630 5 2 1 38.12 2.05 2.3607 1 8 0 39.26 18.54 2.2945 6 4 0 39.44 1.61 2.2845 2 8 0 39.57 8.31 2.2775 5 3 1 39.91 3.16 2.2588 0 7 1 40.23 19.33 2.2413 -1 7 1 40.25 4.82 2.2405 4 7 0 40.34 3.17 2.2355 5 6 0 40.81 1.58 2.2107 -6 1 1 41.40 6.42 2.1809 -2 7 1 41.35 1.69 2.1831 7 2 0 41.57 1.95 2.1723 3 8 0 41.66 1.17 2.1676 -6 2 1 41.80 1.22 2.1606 2 7 1 42.53 1.49 2.1255 -4 6 1 42.74 1.76 2.1152 7 3 0 42.86 7.18 2.1095 6 2 1 43.32 1.76 2.0885 4 6 1 43.35 5.03 2.0872 -3 7 1 43.93 6.14 2.0607 3 7 1 44.09 24.21 2.0537 0 8 1 44.22 9.18 2.0480 6 3 1 44.58 6.29 2.0322 1 8 1 45.04 12.98 2.0126 0 0 2 44.63 13.10 2.0299 7 4 0 44.83 6.25 2.0213 6 6 0 44.93 10.09 2.0173 -6 4 1 45.30 10.41 2.0015 0 1 2 45.50 6.09 1.9932 -1 1 2 46.28 6.65 1.9615 -1 2 2 45.99 1.32 1.9730 -5 6 1 46.26 3.15 1.9622 8 0 0 46.52 2.61 1.9519 8 1 0 46.74 6.72 1.9430 4 7 1 46.72 2.78 1.9440 -7 2 1 46.97 2.03 1.9340 7 5 0 47.25 6.13 1.9231 -6 5 1 47.28 1.96 1.9220 8 2 0 47.59 9.11 1.9103 0 10 0 47.83 2.87 1.9014 3 8 1 47.96 4.96 1.8963 1 10 0 48.00 6.16 1.8950 7 2 1 48.49 1.05 1.8771 -2 3 2 48.34 3.54 1.8822 6 5 1 48.90 1.16 1.8620 -3 2 2 48.77 7.50 1.8670 4 9 0 48.93 3.39 1.8610 1 9 1 49.23 1.43 1.8503 3 1 2 49.65 1.76 1.8357 1 4 2 49.77 5.71 1.8316 -4 8 1 49.72 4.65 1.8334 -7 4 1 49.72 8.50 1.8334 7 6 0 50.13 3.38 1.8193 -3 3 2 49.99 10.23 1.8241 -6 6 1 50.29 3.82 1.8140 -4 0 2 50.15 6.10 1.8185 5 7 1 50.90 10.38 1.7934 2 4 2 50.87 1.08 1.7944 3 10 0 51.13 2.96 1.7859 -8 0 1 51.67 2.42 1.7685 4 0 2 51.37 3.68 1.7782 -8 1 1 51.91 6.68 1.7610 4 1 2 51.88 2.59 1.7618 -7 5 1 51.99 2.32 1.7584 5 9 0 52.36 11.39 1.7470 -2 5 2 52.08 1.04 1.7555 -8 2 1 52.68 4.01 1.7369 9 1 0 53.07 2.36 1.7251 7 5 1 53.32 6.56 1.7176 4 10 0 53.44 4.43 1.7142 8 2 1 53.38 2.43 1.7158 9 2 0 53.91 1.78 1.7001 -3 5 2 53.71 1.78 1.7062 5 8 1 53.80 4.08 1.7034 -4 9 1 54.20 1.61 1.6918 -5 2 2 54.09 1.88 1.6951 6 7 1 54.38 2.84 1.6865 1 6 2 54.47 3.02 1.6841 4 9 1 54.95 1.90 1.6704 8 6 0 55.34 1.51 1.6595 -5 3 2 55.56 5.34 1.6536 2 6 2 55.75 1.72 1.6482 3 11 0 56.12 2.00 1.6383 9 4 0 56.74 1.17 1.6218 -5 9 1 57.31 1.52 1.6071 1 7 2 57.38 4.55 1.6054 3 6 2 57.70 2.60 1.5971 -6 2 2 57.81 1.12 1.5943 -2 7 2 58.54 1.46 1.5761 -4 6 2 58.80 1.46 1.5698 10 0 0 59.27 2.50 1.5584 -3 7 2 59.02 2.00 1.5645 10 1 0 59.67 1.58 1.5490 10 2 0 60.10 1.99 1.5389 0 8 2 60.27 1.01 1.5351 -1 8 2 59.99 1.17 1.5415 7 9 0 60.31 1.76 1.5340 -6 4 2 60.46 2.21 1.5306 -3 11 1 60.94 4.47 1.5196 5 11 0 61.34 3.20 1.5107 -4 7 2 61.11 1.40 1.5160 8 8 0 61.70 1.37 1.5027 -7 2 2 62.16 2.64 1.4929 6 4 2 62.23 2.17 1.4914 -6 5 2 62.58 2.42 1.4837 -4 11 1 62.98 1.47 1.4754 -1 12 1 63.13 3.39 1.4722 1 12 1 63.19 1.22 1.4709 4 11 1 63.30 1.19 1.4686 8 7 1 63.69 2.76 1.4604 0 9 2 64.04 7.37 1.4535 6 5 2 64.22 1.09 1.4498 -7 4 2 64.13 3.66 1.4517 2 12 1 64.11 1.99 1.4520 10 5 0 64.86 1.48 1.4370 7 3 2 64.67 1.13 1.4408 8 9 0 64.71 1.88 1.4399 -10 3 1 65.27 1.07 1.4288 -5 11 1 65.57 1.62 1.4231 11 1 0 66.30 2.83 1.4093 6 6 2 66.19 2.84 1.4113 10 3 1 66.39 3.57 1.4076 8 8 1 66.34 1.08 1.4085 9 8 0 67.06 1.27 1.3951 -5 8 2 67.18 2.23 1.3929 -8 3 2 67.21 1.20 1.3924 -9 7 1 67.58 1.10 1.3855 0 10 2 67.69 3.34 1.3835 8 0 2 67.61 1.36 1.3850 10 4 1 67.97 4.23 1.3786 -10 5 1 68.29 2.08 1.3729 -7 6 2 68.51 1.02 1.3689 9 7 1 68.52 1.63 1.3688 8 10 0 68.65 1.12 1.3665 -8 9 1 68.91 5.48 1.3620 -2 13 1 69.10 3.23 1.3587 4 9 2 69.20 1.45 1.3570 2 13 1 69.41 1.56 1.3534 10 5 1 70.10 1.86 1.3417 0 0 3 69.82 1.08 1.3466 -3 10 2 69.95 2.06 1.3443 2 14 0 70.47 2.26 1.3357 -9 1 2 70.76 1.12 1.3309 5 13 0 71.72 3.44 1.3154 -4 10 2 71.59 1.65 1.3175 10 6 1 72.87 1.05 1.2974 -3 2 3 72.41 2.14 1.3046 -8 10 1 73.60 1.04 1.2863 9 2 2 73.53 1.23 1.2874 8 10 1 74.09 1.36 1.2790 -4 1 3 73.54 1.31 1.2872 -9 9 1 74.13 2.23 1.2784 3 2 3 73.81 1.04 1.2833 -7 8 2 73.89 1.66 1.2821 6 12 1 74.67 2.74 1.2705 -4 2 3 74.12 1.50 1.2786 10 7 1 74.81 1.32 1.2685 2 4 3 74.77 2.35 1.2691 3 11 2 75.10 1.27 1.2643 3 3 3 74.75 1.31 1.2694 1 15 0 75.06 2.26 1.2649 -8 7 2 75.71 2.27 1.2556 -2 5 3 75.58 1.04 1.2575 -3 14 1 75.61 2.00 1.2571 2 15 0 76.34 1.33 1.2468 4 2 3 75.71 1.36 1.2557 -12 0 1 76.54 1.48 1.2440 2 5 3 76.36 1.33 1.2465 -1 12 2 76.47 1.07 1.2450 -8 11 1 76.48 1.08 1.2450 -12 2 1 77.01 1.07 1.2377 10 8 1 77.66 1.06 1.2290 7 12 1 77.56 3.14 1.2302 12 1 1 78.63 1.54 1.2161 -11 7 1 79.14 1.90 1.2096 10 2 2 79.65 1.94 1.2031 -1 7 3 79.12 2.23 1.2098 6 14 0 80.86 1.08 1.1881 -6 3 3 81.16 1.12 1.1845 -8 9 2 82.18 1.77 1.1723 -6 4 3 82.89 1.23 1.1641 1 8 3 82.39 1.63 1.1699 7 13 1 83.31 2.71 1.1593 6 3 3 83.10 1.20 1.1617 10 5 2 84.40 1.10 1.1471 -11 4 2 85.93 1.74 1.1305 -6 6 3 85.50 1.00 1.1351 -9 12 1 86.73 1.61 1.1221 -8 1 3 86.50 1.87 1.1246 -7 14 1 86.89 2.96 1.1205 8 10 2 87.23 1.13 1.1169 -5 13 2 87.65 1.67 1.1127 4 8 3 87.41 2.09 1.1151 2 14 2 87.78 1.06 1.1114 -12 8 1 87.78 1.06 1.1114 -12 8 1 XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.