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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 Powder_meas_from Gu
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.111
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    8.8163 9.897181   0  1  1    2    8.7817  9.935602   -0.0346 -0.038421
   10.2785 8.507346   0  0  2    2   10.2450  8.534785   -0.0335 -0.027439
   12.0691 7.260425   1  1  0    2   12.0482  7.272841   -0.0209 -0.012416
   13.1139 6.689097   1  1  1    2   13.1104  6.690839   -0.0035 -0.001742
   19.5008 4.522746   2  0  0    2   19.4893  4.525365   -0.0115 -0.002619
   20.2484 4.358328   1  2  2    2   20.2645  4.354917    0.0161  0.003411
   21.4702 4.114269   2  1  1    2   21.4488  4.118306   -0.0214 -0.004037
   23.2700 3.801480   2  1  2    2   23.2801  3.799868    0.0101  0.001612
   23.8376 3.712652   1  3  0    2   23.8276  3.714173   -0.0100 -0.001521
   25.3495 3.495511   0  2  4    2   25.3277  3.498452   -0.0218 -0.002940
   26.0292 3.406142   1  3  2    2   26.0330  3.405661    0.0038  0.000481
   27.8095 3.192870   1  0  5    2   27.7973  3.194233   -0.0122 -0.001363
   30.3721 2.930044   3  1  0    2   30.3837  2.928952    0.0116  0.001093
   32.9733 2.705377   3  2  0    2   32.9772  2.705065    0.0039  0.000311
   34.1350 2.616216   0  3  5    2   34.1329  2.616372   -0.0021 -0.000156
   37.9343 2.363234   2  1  6    2   37.9374  2.363051    0.0031  0.000184
   38.7847 2.313501   2  4  3    2   38.7902  2.313185    0.0055  0.000316
   43.2921 2.083116   0  4  6    2   43.3192  2.081879    0.0271  0.001237
   46.6647 1.940475   1  5  5    2   46.6541  1.940892   -0.0106 -0.000417
   50.0445 1.817346   3  4  5    2   50.0498  1.817166    0.0053  0.000181
   52.5829 1.735621   5  2  0    2   52.5846  1.735568    0.0017  0.000053
   68.1844 1.372244   4  5  7    2   68.1764  1.372385   -0.0080 -0.000141

 rmse = 0.00010039467
 
     A =9.051(1)               B =12.219(3)               C =17.070(5)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 1887.7(3)