Manganilvaite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern for R070334 Zotov N, Kockelmann W, Jacobsen S D, Mitov I, Paneva D, Vassileva R D, Bonev I K The Canadian Mineralogist 43 (2005) 1043-1053 Structure and cation order in manganilvaite: a combined X-ray-diffraction, neutron-diffraction and mossbauer study Sample: Ossikovo Pb-Zn skarn, Rhodope Mountains, Bulgaria Sample: single crystal X-ray analysis CELL PARAMETERS: 12.99353 8.852164 5.842728 90.00000 89.94728 90.00000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 2-THETA INTENSITY D-SPACING H K L 12.15 2.49 7.3157 1 1 0 13.68 21.34 6.4968 2 0 0 15.21 22.92 5.8427 0 0 1 16.98 4.87 5.2376 2 1 0 18.24 12.51 4.8763 0 1 1 19.49 40.67 4.5666 1 1 1 20.11 20.66 4.4261 0 2 0 22.84 9.92 3.9014 2 1 1 22.90 6.24 3.8905 3 1 0 24.38 1.30 3.6579 2 2 0 25.29 8.38 3.5281 0 2 1 26.22 1.00 3.4043 -1 2 1 26.21 12.03 3.4053 1 2 1 27.50 6.71 3.2484 4 0 0 27.57 15.35 3.2395 3 1 1 28.88 2.15 3.0956 3 2 0 30.64 38.00 2.9214 0 0 2 31.12 31.39 2.8775 1 3 0 31.56 100.00 2.8380 -4 0 1 31.54 39.87 2.8402 4 0 1 32.78 5.18 2.7347 -3 2 1 32.77 25.12 2.7361 3 2 1 33.06 29.36 2.7126 -1 1 2 33.05 32.51 2.7135 1 1 2 33.39 46.41 2.6866 2 3 0 34.07 1.46 2.6339 0 3 1 34.27 4.04 2.6188 4 2 0 34.79 10.95 2.5812 -1 3 1 34.78 1.37 2.5816 1 3 1 35.22 8.61 2.5505 -2 1 2 35.20 8.14 2.5521 2 1 2 36.86 44.42 2.4406 -2 3 1 36.85 9.68 2.4413 2 3 1 36.89 2.74 2.4386 3 3 0 36.90 6.67 2.4382 0 2 2 37.68 8.88 2.3891 -4 2 1 37.66 39.19 2.3904 4 2 1 38.58 12.32 2.3351 -3 1 2 38.55 10.92 2.3370 3 1 2 39.30 7.50 2.2941 5 1 1 40.10 4.00 2.2500 -3 3 1 41.36 2.58 2.1841 4 3 0 41.41 12.66 2.1816 1 4 0 41.62 9.92 2.1712 -4 0 2 41.58 8.83 2.1732 4 0 2 42.59 1.65 2.1239 -3 2 2 42.56 2.07 2.1253 3 2 2 42.91 32.57 2.1087 -4 1 2 42.88 32.98 2.1105 4 1 2 43.21 17.22 2.0948 2 4 0 43.25 1.75 2.0929 5 2 1 44.21 1.82 2.0498 -1 3 2 44.20 1.63 2.0502 1 3 2 44.34 2.45 2.0439 1 4 1 44.66 1.78 2.0300 -6 0 1 45.86 1.84 1.9798 6 1 1 45.92 3.67 1.9771 -2 3 2 45.90 4.13 1.9779 2 3 2 46.05 6.66 1.9717 -2 4 1 46.05 7.36 1.9721 2 4 1 46.08 5.29 1.9707 3 4 0 46.62 2.59 1.9493 -4 2 2 46.58 2.43 1.9507 4 2 2 46.66 1.22 1.9476 0 0 3 47.84 3.99 1.9021 0 1 3 48.01 6.19 1.8957 -5 1 2 47.97 6.86 1.8974 5 1 2 48.39 3.63 1.8818 -1 1 3 48.78 3.79 1.8676 3 4 1 49.29 6.58 1.8495 -5 3 1 49.27 1.03 1.8503 5 3 1 49.39 4.06 1.8461 6 2 1 49.88 1.69 1.8289 4 4 0 49.99 1.20 1.8250 -2 1 3 50.24 1.82 1.8167 7 1 0 51.27 1.20 1.7826 0 2 3 51.79 2.33 1.7659 -1 2 3 51.85 1.52 1.7640 0 4 2 52.42 3.51 1.7459 6 3 0 52.36 3.90 1.7479 -1 4 2 52.35 3.15 1.7481 1 4 2 52.45 1.77 1.7452 -4 4 1 52.58 2.85 1.7410 -3 1 3 53.55 15.43 1.7118 7 2 0 53.88 1.21 1.7022 -2 4 2 54.14 1.55 1.6944 0 5 1 54.91 14.41 1.6724 -6 3 1 54.89 5.01 1.6731 6 3 1 55.01 4.46 1.6697 -4 0 3 54.96 12.19 1.6710 4 0 3 55.80 2.64 1.6480 -3 2 3 56.11 4.06 1.6394 -2 5 1 56.10 17.05 1.6396 2 5 1 56.34 3.21 1.6334 -3 4 2 56.31 3.31 1.6340 3 4 2 56.68 7.56 1.6242 8 0 0 56.79 8.55 1.6215 -5 3 2 56.75 8.61 1.6225 5 3 2 57.11 3.74 1.6130 1 3 3 58.56 2.70 1.5766 -2 3 3 58.54 10.53 1.5771 2 3 3 59.15 6.67 1.5622 -4 2 3 59.10 1.37 1.5633 4 2 3 59.75 2.66 1.5478 6 4 0 60.03 1.84 1.5413 8 1 1 60.34 1.76 1.5342 -5 1 3 60.75 18.24 1.5248 8 2 0 61.95 17.08 1.4981 -6 3 2 61.90 16.59 1.4991 6 3 2 63.01 1.53 1.4754 0 6 0 63.05 19.93 1.4744 -2 5 2 63.04 19.67 1.4747 2 5 2 63.46 3.08 1.4659 1 6 0 63.72 28.55 1.4607 0 0 4 65.30 1.21 1.4291 -3 5 2 65.27 1.19 1.4295 3 5 2 65.51 4.00 1.4249 9 1 0 65.45 1.13 1.4262 -2 4 3 65.65 1.43 1.4222 7 4 0 65.82 4.24 1.4190 -8 0 2 65.67 1.32 1.4218 -1 6 1 65.76 3.90 1.4201 8 0 2 67.01 1.92 1.3966 3 6 0 67.70 1.94 1.3840 -9 1 1 67.65 1.55 1.3850 -3 4 3 68.00 2.69 1.3785 5 3 3 68.45 7.53 1.3707 6 5 0 69.16 4.10 1.3582 -3 6 1 70.56 4.01 1.3346 6 5 1 71.66 1.00 1.3169 0 6 2 72.58 1.87 1.3024 -1 3 4 72.57 2.23 1.3026 1 3 4 72.77 1.86 1.2995 -6 3 3 72.71 5.32 1.3005 6 3 3 73.68 2.03 1.2856 10 1 0 73.79 7.76 1.2840 -2 5 3 73.85 3.88 1.2831 -2 3 4 73.77 2.11 1.2844 2 5 3 73.82 3.97 1.2835 2 3 4 74.08 1.12 1.2796 8 3 2 74.84 1.69 1.2686 10 0 1 75.00 1.98 1.2662 9 3 1 75.93 2.23 1.2530 -5 6 1 75.91 1.34 1.2533 5 6 1 76.38 4.01 1.2467 10 2 0 76.83 1.43 1.2406 -6 5 2 76.79 1.48 1.2412 6 5 2 77.27 1.19 1.2346 -8 1 3 78.42 1.66 1.2193 6 6 0 80.09 1.28 1.1980 -2 4 4 80.06 1.28 1.1983 2 4 4 81.16 2.67 1.1849 -9 3 2 81.10 2.68 1.1856 9 3 2 81.70 1.79 1.1784 4 7 0 82.84 1.33 1.1651 -10 3 1 82.80 2.71 1.1655 10 3 1 84.12 1.07 1.1505 9 1 3 85.53 2.56 1.1351 3 6 3 86.91 2.90 1.1206 -6 5 3 87.88 2.53 1.1107 -7 2 4 87.79 2.59 1.1116 7 2 4 88.30 1.02 1.1065 0 8 0 88.85 1.62 1.1011 -10 3 2 88.78 1.48 1.1017 10 3 2 89.04 4.37 1.0992 -4 0 5 88.97 1.93 1.0999 4 0 5 89.63 1.27 1.0935 3 2 5 89.63 1.27 1.0935 3 2 5 XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.