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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R040104
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.018
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    8.8884 9.960461   0  0  2    2    8.8795  9.970457   -0.0089 -0.009996
   17.7984 4.984228   0  0  4    2   17.7948  4.985228   -0.0036 -0.001000
   22.9049 3.882407  -1  1  3    2   22.9147  3.880766    0.0098  0.001641
   23.8370 3.732548   0  2  3    2   23.8355  3.732778   -0.0015 -0.000231
   26.8209 3.323403   0  0  6    2   26.8202  3.323486   -0.0007 -0.000083
   27.8751 3.199985   1  1  4    2   27.8784  3.199610    0.0033  0.000374
   29.8873 2.988836   0  2  5    2   29.8960  2.987989    0.0087  0.000847
   31.2698 2.859699   1  1  5    2   31.2680  2.859859   -0.0018 -0.000161
   32.0725 2.789895  -1  1  6    2   32.0676  2.790307   -0.0049 -0.000412
   36.0185 2.492630   0  0  8    2   36.0187  2.492614    0.0002  0.000016
   37.7716 2.380816   1  3  3    2   37.7686  2.381001   -0.0030 -0.000184
   45.4672 1.993975   0  0 10    2   45.4644  1.994091   -0.0028 -0.000116
   65.4921 1.424372   0  0 14    2   65.4932  1.424351    0.0011  0.000021

 rmse = 0.00003639134
 
     A =     5.201(1)          B =     9.022(2)           C =    20.0430(7)      
 Alpha =    90.             Beta =    95.78(1)        Gamma =    90.             
 
 Volume =    935.8(2)