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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060182
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.063
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    8.9056 9.992231   0  0  2    2    8.9194  9.976691    0.0138  0.015540
   17.8314 4.987695   0  0  4    2   17.8291  4.988345   -0.0023 -0.000650
   22.9930 3.875284  -1  1  3    2   22.9870  3.876280   -0.0060 -0.000996
   23.8869 3.731862   0  2  3    2   23.8851  3.732146   -0.0018 -0.000284
   25.5882 3.486850  -1  1  4    2   25.5782  3.488192   -0.0100 -0.001342
   26.8484 3.325591   0  0  6    2   26.8486  3.325564    0.0002  0.000027
   27.9361 3.198236   1  1  4    2   27.9381  3.198015    0.0020  0.000221
   29.9407 2.988060   0  2  5    2   29.9379  2.988335   -0.0028 -0.000276
   31.3230 2.859008   1  1  5    2   31.3219  2.859107   -0.0011 -0.000099
   32.1140 2.790231  -1  1  6    2   32.1238  2.789399    0.0098  0.000832
   36.0319 2.494779   0  0  8    2   36.0409  2.494173    0.0090  0.000606
   37.8386 2.379508   1  3  3    2   37.8395  2.379453    0.0009  0.000056
   45.4861 1.995079   0  0 10    2   45.4799  1.995338   -0.0062 -0.000259
   55.8730 1.645880   1  3  9    2   55.8736  1.645864    0.0006  0.000017

 rmse = 0.00004838203
 
     A =5.190(2)               B =9.018(2)                C =20.055(2)           
 Alpha =90                  Beta =95.76(1)            Gamma =90                  
 
 Volume = 933.9(0)