******************************************************************************
       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 Olivenite__R050532-1__Powder__Xray_Data_XY_Processed__1745[1]
 
 Symmetry constraint is: MONOCLINIC3 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.026
  
 Number of iterations =   3

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   14.8941 5.953308   1  1  0    2   14.9027  5.949899    0.0086  0.003410
   18.1503 4.890429   1  0  1    2   18.1571  4.888618    0.0068  0.001811
   20.6366 4.305763   2  0  0    2   20.6367  4.305744    0.0001  0.000019
   23.9675 3.713729   1  2  0    2   23.9724  3.712987    0.0049  0.000742
   31.8814 2.806878   1  0  2    2   31.8805  2.806956   -0.0009 -0.000078
   33.0413 2.710869   3  1  0    2   33.0474  2.710378    0.0061  0.000491
   34.3036 2.613873   1  3  0    2   34.3020  2.613990   -0.0016 -0.000117
   34.7046 2.584560   3  0  1    2   34.7070  2.584388    0.0024  0.000172
   36.7647 2.444223   2  0  2    2   36.7634  2.444309   -0.0013 -0.000085
   49.9093 1.826622   2 -3  2    2   49.9093  1.826622    0.0000  0.000000
   52.4873 1.742766   4  0  2    2   52.4825  1.742914   -0.0048 -0.000148
   54.4105 1.685592   5  1  0    2   54.4039  1.685782   -0.0066 -0.000190
   73.2040 1.292261   6  0  2    2   73.2084  1.292194    0.0044  0.000067

 rmse = 0.00004630082
 
     A =8.6115(4)              B =8.230(1)                C =5.9382(7)           
 Alpha =90.12(2)            Beta =90                  Gamma =90                  
 
 Volume = 420.87(8)