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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050391
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.003
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   20.4325 4.343624   1  1  0    2   20.4301  4.344119   -0.0024 -0.000495
   26.2758 3.389307   1  2  0    2   26.2769  3.389163    0.0011  0.000144
   33.9686 2.637203   1  3  0    2   33.9754  2.636689    0.0068  0.000514
   36.3288 2.471085   0  2  1    2   36.3188  2.471743   -0.0100 -0.000658
   40.8574 2.207014   1  2  1    2   40.8587  2.206945    0.0013  0.000069
   47.0702 1.929152   2  3  0    2   47.0742  1.928997    0.0040  0.000155
   57.2698 1.607425   2  3  1    2   57.2676  1.607483   -0.0022 -0.000057
   61.7441 1.501235   1  5  1    2   61.7504  1.501096    0.0063  0.000139
   62.2698 1.489817   2  5  0    2   62.2624  1.489977   -0.0074 -0.000160
   65.4811 1.424305   3  0  1    2   65.4826  1.424276    0.0015  0.000029

 rmse = 0.00006572863
 
     A =4.9009(4)              B =9.3839(8)               C =2.9080(5)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 133.74(2)