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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060072
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.052
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   32.0777 2.792359   3  3  0    2   32.0686  2.793129   -0.0091 -0.000770
   38.0206 2.367842   3  5  0    2   38.0159  2.368127   -0.0047 -0.000285
   28.6979 3.113664   3  1  0    2   28.6928  3.114206   -0.0051 -0.000542
   69.1662 1.357976   5  1  2    2   69.1640  1.358014   -0.0022 -0.000039
   32.7666 2.735114  -3  3  1    2   32.7625  2.735451   -0.0041 -0.000336
   21.2427 4.189229   2  2  0    2   21.2403  4.189693   -0.0024 -0.000464
   26.5211 3.364582   1  3  1    2   26.5195  3.364776   -0.0016 -0.000194
   19.9169 4.465729   0  4  0    2   19.9155  4.466042   -0.0014 -0.000313
   57.5798 1.600745   1 11  0    2   57.5802  1.600735    0.0004  0.000010
   68.7004 1.366049  -5  5  3    2   68.7000  1.366056   -0.0004 -0.000007
   48.2350 1.887041   5  1  0    2   48.2371  1.886964    0.0021  0.000077
   27.4544 3.252070   2  4  0    2   27.4569  3.251779    0.0025  0.000291
   44.4371 2.039288   2  0  2    2   44.4406  2.039135    0.0035  0.000152
   33.3600 2.687730   1  5  1    2   33.3641  2.687411    0.0041  0.000319
   50.4790 1.808203   5  3  0    2   50.4851  1.807999    0.0061  0.000204
   10.5926 8.385871   1  1  0    2   10.6008  8.379387    0.0082  0.006484
   18.0957 4.912152  -1  1  1    2   18.1039  4.909927    0.0082  0.002225
    9.9374 8.940162   0  2  0    2    9.9464  8.932083    0.0090  0.008079

 rmse = 0.00003860750
 
     A =9.8384(5)              B =17.8642(9)              C =5.3105(3)           
 Alpha =90                  Beta =105.339(3)          Gamma =90                  
 
 Volume = 900.10(6)