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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050224
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.033
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.9556 8.906347   1  0  0    2    9.9661  8.896949    0.0105  0.009399
   16.7868 5.287195  -1  0  2    2   16.7888  5.286566    0.0020  0.000629
   19.4650 4.564128  -2  0  2    2   19.4652  4.564086    0.0002  0.000042
   19.9766 4.448190   2  0  0    2   19.9753  4.448474   -0.0013 -0.000285
   26.6157 3.350408   2  1  0    2   26.6187  3.350035    0.0030  0.000373
   31.5235 2.838548  -3  1  2    2   31.5181  2.839026   -0.0054 -0.000477
   31.7266 2.820820   1  1  2    2   31.7302  2.820504    0.0036  0.000316
   33.9231 2.642853  -2  0  4    2   33.9174  2.643283   -0.0057 -0.000430
   34.3363 2.611958  -3  1  3    2   34.3371  2.611899    0.0008  0.000059
   35.2541 2.545970   0  2  0    2   35.2555  2.545872    0.0014  0.000098
   45.7519 1.982830  -5  0  4    2   45.7541  1.982739    0.0022  0.000091
   47.0365 1.931591   3  2  0    2   47.0332  1.931719   -0.0033 -0.000128
   47.9679 1.896211   3  1  2    2   47.9683  1.896197    0.0004  0.000014
   49.7095 1.833734  -2  2  4    2   49.7112  1.833674    0.0017  0.000060

 rmse = 0.00002884280
 
     A =    10.3931(6)         B =     5.0917(3)          C =    10.5736(7)      
 Alpha =    90.             Beta =   121.125(4)       Gamma =    90.             
 
 Volume =    478.99(3)