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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 Phosphosiderite__R070519-9__Powder__Xray_Data_XY_Processed__9551[1]
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  0.710710
 Wavelength #2 =  0.709270
 Wavelength #3 =  0.713590
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.010
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    6.2672 6.497665   0  1  1    2    6.2497  6.515849   -0.0175 -0.018184
    8.3031 4.904412   0  2  0    2    8.3052  4.903174    0.0021  0.001238
    9.3433 4.358839   0  0  2    2    9.3421  4.359414   -0.0012 -0.000576
    9.9791 4.081486   1  1  1    2    9.9734  4.083828   -0.0057 -0.002342
   11.3119 3.601472   1  2  0    2   11.3220  3.598261    0.0101  0.003211
   19.1970 2.127915   0  1  4    2   19.1982  2.127778    0.0012  0.000137
   19.7538 2.068476  -2  2  2    2   19.7531  2.068552   -0.0007 -0.000076
   35.0360 1.178488   0  7  4    2   35.0358  1.178495   -0.0002 -0.000007

 rmse = 0.00010358494
 
     A =5.298(3)               B =9.806(1)                C =8.720(2)            
 Alpha =90                  Beta =91.02(6)            Gamma =90                  
 
 Volume = 453.0(3)