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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 R060915
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.023
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.8718 8.973374   0  2  0    2    9.8674  8.977376   -0.0044 -0.004002
   10.4767 8.455448   1  1  0    2   10.4809  8.452037    0.0042  0.003411
   19.7883 4.488024   0  4  0    2   19.7853  4.488688   -0.0030 -0.000664
   26.3177 3.386511   1  3  1    2   26.3121  3.387214   -0.0056 -0.000704
   27.2256 3.275510   2  4  0    2   27.2273  3.275303    0.0017  0.000207
   28.3882 3.143844   3  1  0    2   28.3872  3.143950   -0.0010 -0.000106
   30.2221 2.956973   2  2  1    2   30.2293  2.956289    0.0072  0.000684
   31.7565 2.817408   3  3  0    2   31.7572  2.817346    0.0007  0.000062
   32.7758 2.732018  -3  3  1    2   32.7786  2.731789    0.0028  0.000229
   33.1283 2.703729   1  5  1    2   33.1277  2.703775   -0.0006 -0.000047
   34.7310 2.582460   0  6  1    2   34.7297  2.582553   -0.0013 -0.000093
   35.4825 2.529432  -2  0  2    2   35.4834  2.529370    0.0009  0.000063
   37.6827 2.386556   3  5  0    2   37.6877  2.386253    0.0050  0.000303
   38.5640 2.333987  -3  5  1    2   38.5707  2.333595    0.0067  0.000392
   39.3796 2.287477  -1  7  1    2   39.3756  2.287699   -0.0040 -0.000222
   41.7387 2.163406   2  6  1    2   41.7412  2.163281    0.0025  0.000124
   44.0675 2.054268   2  0  2    2   44.0675  2.054267    0.0000  0.000001
   44.7677 2.023734   3  5  1    2   44.7635  2.023913   -0.0042 -0.000179
   47.7267 1.904879   5  1  0    2   47.7193  1.905155   -0.0074 -0.000276
   49.0762 1.855584  -1  9  1    2   49.0681  1.855872   -0.0081 -0.000288
   55.4556 1.656185   4  6  1    2   55.4585  1.656105    0.0029  0.000080
   56.1308 1.637845   4  8  0    2   56.1380  1.637652    0.0072  0.000193
   57.7150 1.596581   6  0  0    2   57.7125  1.596643   -0.0025 -0.000062
   60.2572 1.535132  -6  0  2    2   60.2568  1.535142   -0.0004 -0.000009
   64.6581 1.440826  -6  6  1    2   64.6587  1.440814    0.0006  0.000012
   68.1966 1.374403   5  1  2    2   68.1967  1.374401    0.0001  0.000002

 rmse = 0.00004247970
 
     A =9.8859(3)              B =17.9548(9)              C =5.2756(4)           
 Alpha =90                  Beta =104.294(3)          Gamma =90                  
 
 Volume = 907.42(7)