Raspite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern of R050567 Fujita T, Kawada I, Kato K Acta Crystallographica B33 (1977) 162-164 Raspite from Broken Hill Locality: Broken Hill NSW, Australia CELL PARAMETERS: 13.5730 4.9800 5.5630 90.000 107.650 90.000 SPACE GROUP: P2_1/a ATOM X Y Z OCCUPANCY ISO(B) Pb 0.14961 0.19405 0.16670 1.000 0.973 W 0.07708 0.74944 0.61185 1.000 0.551 O 0.01630 0.05150 0.72900 1.000 0.680 O 0.05950 0.43460 0.38820 1.000 0.950 O 0.15100 0.61480 0.90000 1.000 1.420 O 0.19030 0.88290 0.53860 1.000 1.100 X-RAY WAVELENGTHS: 1.540562 1.544390 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 11 +/- 4 +/- 4 MAX. ABS. INTENSITY / VOLUME**2: 231.2247136 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 13.68 / 13.72 6.72 / 3.36 6.4670 2 0 0 16.71 / 16.75 4.93 / 2.46 5.3011 0 0 1 18.12 / 18.17 3.47 / 1.73 4.8908 -2 0 1 19.08 / 19.13 3.28 / 1.64 4.6474 1 1 0 24.03 / 24.09 5.39 / 2.69 3.7002 -1 1 1 24.51 / 24.57 100.00 / 50.00 3.6296 0 1 1 24.71 / 24.78 17.61 / 8.80 3.5995 2 0 1 25.51 / 25.57 38.49 / 19.25 3.4894 -2 1 1 27.34 / 27.41 2.83 / 1.42 3.2595 3 1 0 27.56 / 27.63 22.24 / 11.12 3.2335 4 0 0 27.59 / 27.66 26.23 / 13.12 3.2300 -4 0 1 30.62 / 30.70 30.03 / 15.01 2.9172 2 1 1 32.36 / 32.44 28.97 / 14.48 2.7642 -2 0 2 33.00 / 33.09 35.52 / 17.76 2.7120 4 1 0 33.03 / 33.11 34.37 / 17.19 2.7099 -4 1 1 33.79 / 33.88 1.06 / 0.53 2.6506 0 0 2 36.04 / 36.13 20.67 / 10.33 2.4900 0 2 0 36.65 / 36.74 4.81 / 2.40 2.4500 4 0 1 36.72 / 36.82 2.48 / 1.24 2.4454 -4 0 2 36.73 / 36.82 4.11 / 2.05 2.4451 1 2 0 38.27 / 38.37 3.57 / 1.79 2.3497 -5 1 1 40.06 / 40.16 1.37 / 0.68 2.2490 -6 0 1 40.47 / 40.58 11.66 / 5.83 2.2270 2 0 2 40.62 / 40.73 1.46 / 0.73 2.2190 -2 2 1 40.96 / 41.07 3.15 / 1.58 2.2015 1 1 2 41.02 / 41.13 4.13 / 2.06 2.1983 4 1 1 41.09 / 41.19 3.67 / 1.84 2.1950 -4 1 2 41.51 / 41.62 4.45 / 2.22 2.1734 1 2 1 42.78 / 42.89 5.00 / 2.50 2.1122 -3 2 1 44.19 / 44.31 3.66 / 1.83 2.0478 2 2 1 44.53 / 44.65 18.32 / 9.16 2.0330 2 1 2 45.44 / 45.56 3.15 / 1.58 1.9944 -6 0 2 45.83 / 45.95 4.91 / 2.46 1.9783 6 1 0 45.96 / 46.08 8.63 / 4.32 1.9728 4 2 0 45.98 / 46.10 8.48 / 4.24 1.9720 -4 2 1 47.85 / 47.98 1.51 / 0.75 1.8993 3 2 1 49.17 / 49.30 13.08 / 6.54 1.8515 -6 1 2 49.19 / 49.32 2.96 / 1.48 1.8509 -1 2 2 49.21 / 49.34 19.43 / 9.72 1.8501 -2 2 2 50.25 / 50.38 10.21 / 5.10 1.8142 6 0 1 50.86 / 50.99 3.20 / 1.60 1.7939 5 2 0 52.35 / 52.49 4.79 / 2.40 1.7464 4 2 1 52.40 / 52.54 3.81 / 1.91 1.7447 -4 2 2 52.65 / 52.79 16.08 / 8.04 1.7370 -2 1 3 54.00 / 54.15 9.89 / 4.94 1.6966 -8 0 1 55.10 / 55.25 4.03 / 2.02 1.6653 0 1 3 55.30 / 55.44 6.50 / 3.25 1.6600 2 2 2 55.79 / 55.94 1.07 / 0.53 1.6465 1 3 0 56.39 / 56.55 4.51 / 2.26 1.6303 -6 0 3 57.96 / 58.12 2.96 / 1.48 1.5899 -1 3 1 58.09 / 58.25 3.78 / 1.89 1.5866 2 0 3 58.19 / 58.35 4.09 / 2.04 1.5841 0 3 1 58.68 / 58.84 1.45 / 0.72 1.5719 -2 3 1 59.32 / 59.48 1.26 / 0.63 1.5566 -6 2 2 59.63 / 59.79 5.52 / 2.76 1.5493 -6 1 3 59.63 / 59.80 2.71 / 1.36 1.5491 3 3 0 60.12 / 60.29 8.18 / 4.09 1.5378 8 1 0 60.19 / 60.35 6.82 / 3.41 1.5362 -8 1 2 61.26 / 61.43 2.11 / 1.06 1.5118 2 1 3 61.46 / 61.63 4.23 / 2.11 1.5074 2 3 1 62.88 / 63.05 5.47 / 2.74 1.4768 4 3 0 62.90 / 63.07 3.77 / 1.89 1.4764 -4 3 1 63.38 / 63.56 7.05 / 3.52 1.4663 6 2 1 63.96 / 64.13 1.15 / 0.57 1.4545 -7 2 2 64.42 / 64.60 1.16 / 0.58 1.4452 3 3 1 66.28 / 66.47 1.56 / 0.78 1.4090 -5 3 1 66.30 / 66.49 8.61 / 4.30 1.4086 6 1 2 66.45 / 66.63 1.06 / 0.53 1.4058 -3 3 2 66.65 / 66.84 7.43 / 3.72 1.4021 -8 2 1 67.63 / 67.82 2.05 / 1.02 1.3840 4 0 3 67.67 / 67.86 1.09 / 0.55 1.3834 -2 0 4 67.74 / 67.93 2.90 / 1.45 1.3821 -4 0 4 68.14 / 68.33 1.73 / 0.87 1.3750 1 3 2 68.77 / 68.97 4.08 / 2.04 1.3639 -6 2 3 70.29 / 70.49 2.96 / 1.48 1.3381 2 2 3 70.73 / 70.93 1.95 / 0.97 1.3309 2 3 2 70.85 / 71.05 1.19 / 0.60 1.3289 -5 3 2 71.07 / 71.28 2.09 / 1.04 1.3253 0 0 4 71.28 / 71.49 1.37 / 0.68 1.3219 -6 0 4 73.51 / 73.73 2.30 / 1.15 1.2872 -10 1 2 73.95 / 74.16 2.43 / 1.22 1.2807 0 1 4 74.16 / 74.37 1.19 / 0.59 1.2776 -6 1 4 74.27 / 74.49 1.97 / 0.98 1.2759 -6 3 2 75.95 / 76.17 1.69 / 0.85 1.2519 10 1 0 76.86 / 77.09 1.09 / 0.54 1.2393 1 4 0 76.97 / 77.20 2.91 / 1.46 1.2378 -10 0 3 77.06 / 77.29 2.98 / 1.49 1.2365 -2 3 3 77.29 / 77.52 1.18 / 0.59 1.2334 -3 3 3 79.10 / 79.33 2.35 / 1.17 1.2097 4 2 3 79.20 / 79.43 2.51 / 1.25 1.2084 -4 2 4 79.88 / 80.12 1.03 / 0.51 1.1998 6 0 3 79.94 / 80.18 1.30 / 0.65 1.1990 1 4 1 80.80 / 81.05 1.05 / 0.52 1.1885 -3 4 1 80.89 / 81.13 1.45 / 0.73 1.1874 -8 1 4 81.75 / 82.00 1.03 / 0.51 1.1770 10 0 1 82.36 / 82.61 2.24 / 1.12 1.1699 0 2 4 82.56 / 82.81 1.38 / 0.69 1.1676 -6 2 4 82.94 / 83.19 1.30 / 0.65 1.1631 -6 3 3 83.37 / 83.63 1.57 / 0.79 1.1582 8 3 0 84.51 / 84.77 2.77 / 1.39 1.1455 10 1 1 85.46 / 85.73 1.43 / 0.72 1.1352 -2 4 2 86.73 / 87.00 1.04 / 0.52 1.1218 5 4 0 88.05 / 88.32 3.03 / 1.51 1.1084 -10 2 3 88.90 / 89.18 2.05 / 1.03 1.0999 6 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.