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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060313
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.122
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   37.8527 2.382231  -3  3  1    2   37.8439  2.382765   -0.0088 -0.000534
   24.6930 3.620044  -1  3  1    2   24.6874  3.620862   -0.0056 -0.000818
   22.6690 3.940224   1  1  1    2   22.6636  3.941164   -0.0054 -0.000940
   32.4436 2.767478  -1  3  2    2   32.4391  2.767854   -0.0045 -0.000375
   38.8818 2.321317  -1  1  3    2   38.8792  2.321465   -0.0026 -0.000149
   29.9378 2.994113   1  3  1    2   29.9364  2.994255   -0.0014 -0.000141
   35.2999 2.549036   1  1  2    2   35.2996  2.549055   -0.0003 -0.000018
   46.1419 1.970582   2  2  2    2   46.1419  1.970582    0.0000  0.000000
   41.6889 2.170808   0  6  0    2   41.6894  2.170783    0.0005  0.000025
   27.0146 3.312566   2  2  0    2   27.0158  3.312424    0.0012  0.000142
   37.2218 2.421281  -1  5  1    2   37.2237  2.421160    0.0019  0.000121
   21.1748 4.216383  -2  0  1    2   21.1767  4.215999    0.0019  0.000383
   42.5907 2.126775   2  4  1    2   42.5927  2.126679    0.0020  0.000096
   25.2612 3.539496  -2  2  1    2   25.2641  3.539100    0.0029  0.000396
   45.2915 2.005686  -4  2  2    2   45.2948  2.005549    0.0033  0.000137
   25.8189 3.463928  -1  1  2    2   25.8238  3.463275    0.0049  0.000653
   23.6249 3.782087   1  3  0    2   23.6306  3.781188    0.0057  0.000899
   27.7086 3.230787   0  0  2    2   27.7157  3.229975    0.0071  0.000812

 rmse = 0.00003491790
 
     A =8.5602(6)              B =13.0247(8)              C =7.1867(6)           
 Alpha =90                  Beta =115.990(6)          Gamma =90                  
 
 Volume = 720.25(6)