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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060524
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  0.710710
 Wavelength #2 =  0.709270
 Wavelength #3 =  0.713590
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.053
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    7.5448 5.428464   0  1  0    2    7.5787  5.404070    0.0339  0.024395
    8.5493 4.787619   1  1  0    2    8.5872  4.766394    0.0379  0.021225
   11.0792 3.691407   2  1  0    2   11.0759  3.692524   -0.0033 -0.001117
   15.1939 2.691885   2  1  2    2   15.1974  2.691266    0.0035  0.000619
   16.1579 2.531721   4  0  0    2   16.1779  2.528603    0.0200  0.003118
   17.1684 2.383261   2  2  0    2   17.1689  2.383197    0.0005  0.000064
   20.1188 2.035667   2  2  2    2   20.0968  2.037883   -0.0220 -0.002216
   20.7345 1.975693   4  1  2    2   20.7009  1.978874   -0.0336 -0.003181
   23.6333 1.735643   2  1  4    2   23.6435  1.734905    0.0102  0.000738
   24.5624 1.670797   4  2  2    2   24.5579  1.671100   -0.0045 -0.000303
   37.1363 1.115235   8  1  3    2   37.1710  1.114229    0.0347  0.001007
   41.4770 1.002734   9  2  2    2   41.4534  1.003281   -0.0236 -0.000547
   43.9170 0.949483   2  1  8    2   43.9104  0.949618   -0.0066 -0.000135
   47.4888 0.881670   4  4  6    2   47.4957  0.881550    0.0069  0.000120

 rmse = 0.00067141397
 
     A =10.114(3)              B =5.404(4)                C =7.861(3)            
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 429.7(2)