Tintinaite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from single crystal data of R110163 Miehe G Nature Physical Science 231 (1971) 133-134 Crystal structure of kobellite Locality: Korunka mine, Spissko-Gemerske Rudohorie Mountains, Czechoslovakia _database_code_amcsd 0014683 CELL PARAMETERS: 34.0010 22.3110 4.0335 90.000 90.013 90.000 SPACE GROUP: Pnnm ATOM X Y Z OCCUPANCY ISO(B) Cu 0.13070 0.33540 0.50000 0.444 3.500 Fe 0.13070 0.33540 0.50000 0.556 3.500 Pb 0.27360 0.03520 0.50000 1.000 2.700 Pb 0.15560 0.13220 0.50000 1.000 3.100 Pb 0.06390 0.24660 0.50000 1.000 2.800 Pb 0.26750 0.37200 0.00000 1.000 3.800 Pb 0.45820 0.36210 0.00000 1.000 2.800 Pb 0.11390 0.43820 0.00000 1.000 3.500 Bi 0.05270 0.04510 0.00000 0.333 2.400 Sb 0.05270 0.04510 0.00000 0.667 2.400 Bi 0.43810 0.04400 0.00000 0.833 2.400 Sb 0.43810 0.04400 0.00000 0.167 2.400 Bi 0.32680 0.14040 0.00000 0.556 2.000 Sb 0.32680 0.14040 0.00000 0.444 2.000 Bi 0.48730 0.15020 0.50000 0.667 2.500 Sb 0.48730 0.15020 0.50000 0.333 2.500 Bi 0.23390 0.24120 0.00000 0.556 1.900 Sb 0.23390 0.24120 0.00000 0.444 1.900 Bi 0.39500 0.25510 0.50000 0.500 2.000 Sb 0.39500 0.25510 0.50000 0.500 2.000 Bi 0.36690 0.45470 0.50000 0.500 2.600 Sb 0.36690 0.45470 0.50000 0.500 2.600 S 0.50000 0.00000 0.50000 1.000 1.800 S 0.13280 0.04590 0.50000 1.000 2.100 S 0.37810 0.08540 0.50000 1.000 1.100 S 0.23700 0.09530 0.00000 1.000 1.200 S 0.05400 0.11800 0.00000 1.000 1.200 S 0.13890 0.20240 0.00000 1.000 1.000 S 0.28380 0.18220 0.50000 1.000 1.500 S 0.44930 0.19970 0.00000 1.000 1.500 S 0.48900 0.29410 0.50000 1.000 1.100 S 0.35380 0.29650 0.00000 1.000 1.400 S 0.20770 0.28730 0.50000 1.000 1.700 S 0.08740 0.31580 0.00000 1.000 1.300 S 0.03330 0.40090 0.50000 1.000 2.300 S 0.18710 0.39140 0.50000 1.000 1.100 S 0.36690 0.38140 0.50000 1.000 1.700 S 0.28460 0.44990 0.00000 1.000 1.300 S 0.45750 0.44820 0.00000 1.000 1.000 S 0.15320 0.49540 0.50000 1.000 2.100 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 31 +/- 20 +/- 3 MAX. ABS. INTENSITY / VOLUME**2: 38.41509812 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 5.20 6.01 17.0005 2 0 0 11.13 1.44 7.9504 3 2 0 12.18 1.87 7.2652 1 3 0 12.99 2.10 6.8136 2 3 0 13.09 5.69 6.7611 4 2 0 14.24 2.60 6.2179 3 3 0 15.26 5.65 5.8064 5 2 0 15.64 14.44 5.6668 6 0 0 16.14 4.91 5.4924 6 1 0 18.70 3.65 4.7461 7 1 0 19.03 2.89 4.6634 4 4 0 19.70 73.55 4.5074 6 3 0 19.94 32.79 4.4534 7 2 0 20.60 42.53 4.3126 5 4 0 20.90 4.33 4.2501 8 0 0 21.85 10.83 4.0667 7 3 0 22.36 68.50 3.9752 6 4 0 22.40 6.07 3.9692 0 1 1 22.50 7.38 3.9509 4 5 0 22.55 2.67 3.9425 1 1 1 23.01 16.13 3.8654 2 1 1 23.60 6.72 3.7699 1 2 1 23.75 14.70 3.7463 -3 1 1 23.75 14.70 3.7458 3 1 1 23.85 3.98 3.7307 5 5 0 23.89 11.97 3.7249 9 1 0 23.93 2.58 3.7185 0 6 0 24.04 11.47 3.7023 2 2 1 24.12 2.27 3.6901 8 3 0 24.75 3.81 3.5973 3 2 1 24.75 10.01 3.5967 -4 1 1 24.76 10.01 3.5961 4 1 1 24.88 2.77 3.5783 9 2 0 25.12 11.50 3.5456 0 3 1 25.21 3.97 3.5332 3 6 0 25.25 1.57 3.5266 1 3 1 25.41 31.67 3.5058 6 5 0 25.66 33.61 3.4711 2 3 1 25.68 2.98 3.4695 -5 0 1 25.68 2.98 3.4688 5 0 1 25.72 4.88 3.4642 -4 2 1 25.72 4.87 3.4637 4 2 1 25.99 12.50 3.4283 -5 1 1 26.00 12.49 3.4276 5 1 1 26.16 4.03 3.4068 4 6 0 26.21 24.00 3.4001 10 0 0 26.34 66.88 3.3841 3 3 1 26.52 7.12 3.3613 10 1 0 27.14 5.35 3.2861 7 5 0 27.25 3.02 3.2726 4 3 1 27.34 100.00 3.2626 5 6 0 27.41 6.53 3.2535 1 4 1 27.42 2.68 3.2524 10 2 0 27.79 12.52 3.2098 2 4 1 28.31 42.10 3.1525 -6 2 1 28.32 42.07 3.1519 6 2 1 28.39 24.96 3.1442 -5 3 1 28.39 24.95 3.1437 5 3 1 28.42 48.50 3.1406 3 4 1 28.49 1.57 3.1327 2 7 0 28.54 1.53 3.1279 9 4 0 28.71 31.09 3.1089 6 6 0 28.77 2.49 3.1034 -7 0 1 28.77 2.49 3.1027 7 0 1 28.87 1.45 3.0923 10 3 0 29.01 1.32 3.0775 8 5 0 29.17 18.74 3.0618 11 1 0 29.27 1.41 3.0509 4 4 1 29.86 5.57 2.9922 0 5 1 29.98 3.97 2.9808 1 5 1 30.00 15.37 2.9788 11 2 0 30.34 8.42 2.9461 5 4 1 30.80 1.30 2.9032 10 4 0 30.82 17.20 2.9012 -8 1 1 30.83 17.18 2.9005 8 1 1 30.99 3.73 2.8860 5 7 0 31.34 14.60 2.8543 11 3 0 31.58 3.06 2.8334 12 0 0 31.60 21.91 2.8315 6 4 1 31.61 1.60 2.8303 -8 2 1 31.62 1.60 2.8297 8 2 1 31.70 1.41 2.8226 4 5 1 31.84 11.82 2.8108 12 1 0 32.09 6.08 2.7889 0 8 0 32.20 1.90 2.7795 1 8 0 32.22 18.01 2.7780 6 7 0 32.47 48.61 2.7576 -9 0 1 32.48 48.57 2.7570 9 0 1 32.53 2.31 2.7521 2 8 0 32.61 8.09 2.7462 12 2 0 33.13 6.02 2.7036 11 4 0 33.19 1.84 2.6993 2 6 1 33.47 1.34 2.6770 -9 2 1 33.48 1.34 2.6765 9 2 1 33.63 3.97 2.6648 7 7 0 33.72 25.32 2.6578 3 6 1 33.83 5.07 2.6499 4 8 0 33.85 27.36 2.6478 12 3 0 34.46 38.74 2.6028 4 6 1 34.69 7.77 2.5856 -9 3 1 34.70 7.76 2.5851 9 3 1 34.74 3.89 2.5825 -10 1 1 34.75 3.89 2.5819 10 1 1 35.25 1.24 2.5464 13 2 0 35.32 4.37 2.5409 11 5 0 35.38 5.90 2.5368 5 6 1 35.45 17.48 2.5321 -10 2 1 35.46 17.47 2.5316 10 2 1 35.54 1.13 2.5262 12 4 0 35.91 9.57 2.5008 0 7 1 36.01 2.06 2.4940 1 7 1 36.31 3.58 2.4742 2 7 1 36.34 3.54 2.4724 1 9 0 36.34 4.45 2.4720 9 4 1 36.41 4.33 2.4673 13 3 0 36.61 13.24 2.4543 10 3 1 36.63 2.90 2.4531 2 9 0 36.73 2.28 2.4469 8 5 1 36.80 68.74 2.4421 3 7 1 36.85 2.24 2.4390 -11 1 1 36.86 2.23 2.4385 11 1 1 37.17 3.72 2.4186 7 8 0 37.49 24.11 2.3992 4 7 1 37.53 4.55 2.3964 -11 2 1 37.54 4.55 2.3959 11 2 1 37.76 2.17 2.3826 7 6 1 37.85 2.63 2.3770 11 6 0 38.00 2.87 2.3680 13 4 0 38.19 5.40 2.3565 10 4 1 38.37 1.13 2.3458 9 5 1 39.37 10.31 2.2888 1 8 1 39.65 1.58 2.2734 2 8 1 39.70 1.09 2.2703 12 2 1 39.96 3.20 2.2564 13 5 0 40.10 5.73 2.2484 3 8 1 40.14 1.95 2.2464 10 5 1 40.15 8.08 2.2460 11 4 1 40.19 1.03 2.2437 9 8 0 40.43 26.93 2.2311 0 10 0 40.51 3.47 2.2267 14 4 0 40.52 1.62 2.2263 1 10 0 40.57 7.19 2.2235 7 7 1 40.61 2.46 2.2213 15 2 0 40.66 4.22 2.2189 11 7 0 40.74 2.66 2.2150 9 6 1 40.74 4.05 2.2148 4 8 1 40.79 1.80 2.2121 2 10 0 41.65 4.27 2.1683 15 3 0 41.90 2.22 2.1563 10 8 0 42.25 6.78 2.1393 13 6 0 42.42 4.19 2.1308 10 6 1 42.51 6.72 2.1264 6 8 1 42.70 12.56 2.1176 12 7 0 43.39 11.30 2.0854 9 7 1 43.59 5.36 2.0763 3 9 1 43.60 2.27 2.0760 6 10 0 43.67 2.83 2.0726 9 9 0 44.22 1.96 2.0480 11 6 1 44.76 2.88 2.0247 1 11 0 44.83 1.11 2.0219 13 7 0 44.94 8.66 2.0170 5 9 1 44.95 68.22 2.0168 0 0 2 45.00 4.90 2.0147 10 7 1 45.25 2.13 2.0038 14 3 1 45.27 3.92 2.0031 10 9 0 45.54 2.67 1.9921 17 1 0 45.64 5.48 1.9876 12 8 0 45.69 1.63 1.9858 16 4 0 46.11 6.59 1.9686 15 1 1 46.13 1.81 1.9676 12 6 1 46.30 4.32 1.9609 9 8 1 46.59 3.57 1.9496 14 4 1 46.68 2.68 1.9460 15 2 1 46.72 1.40 1.9443 11 7 1 46.91 4.51 1.9369 7 9 1 46.95 1.61 1.9355 15 6 0 47.38 3.37 1.9186 16 5 0 47.61 13.64 1.9100 15 3 1 47.83 4.63 1.9017 10 8 1 47.87 1.33 1.9001 6 0 2 48.11 3.32 1.8914 8 9 1 48.14 2.41 1.8901 13 6 1 48.17 6.26 1.8889 18 0 0 48.59 10.64 1.8736 16 1 1 48.81 2.53 1.8657 12 9 0 48.82 1.80 1.8654 10 10 0 48.89 32.44 1.8628 15 4 1 48.99 3.35 1.8593 0 12 0 49.33 1.06 1.8472 15 7 0 49.37 5.63 1.8459 6 10 1 49.40 1.26 1.8450 16 6 0 49.48 2.16 1.8422 11 8 1 49.51 10.05 1.8410 6 3 2 49.62 4.42 1.8373 7 2 2 49.81 6.84 1.8308 18 3 0 49.81 1.71 1.8305 8 11 0 49.92 6.48 1.8270 5 4 2 50.24 4.62 1.8158 14 6 1 50.37 1.53 1.8115 7 10 1 50.45 1.25 1.8091 11 10 0 50.51 1.97 1.8069 7 3 2 50.74 1.52 1.7992 13 9 0 50.76 12.38 1.7986 6 4 2 50.83 1.16 1.7963 4 5 2 50.89 6.85 1.7942 10 9 1 51.04 4.61 1.7894 3 11 1 51.14 2.81 1.7863 17 1 1 51.27 2.98 1.7818 16 4 1 51.51 4.86 1.7742 8 10 1 51.53 2.15 1.7737 9 1 2 51.57 3.03 1.7723 4 11 1 51.74 2.92 1.7669 19 2 0 52.33 6.74 1.7482 6 5 2 52.43 8.14 1.7451 15 6 1 52.52 1.30 1.7424 14 7 1 52.53 2.82 1.7422 17 3 1 52.61 2.45 1.7395 18 5 0 52.72 1.91 1.7364 7 12 0 52.77 5.07 1.7347 10 0 2 52.78 16.83 1.7345 9 10 1 52.94 1.46 1.7295 10 1 2 53.29 1.15 1.7190 7 5 2 53.41 23.39 1.7155 5 6 2 53.74 1.23 1.7058 18 1 1 54.08 5.09 1.6958 11 11 0 54.17 4.95 1.6932 10 10 1 54.21 8.06 1.6920 6 6 2 54.48 4.71 1.6844 11 1 2 54.62 3.18 1.6802 2 12 1 54.64 3.35 1.6796 15 7 1 54.98 4.06 1.6702 11 2 2 55.09 2.03 1.6669 8 11 1 55.44 1.04 1.6573 20 3 0 55.48 1.94 1.6562 4 12 1 55.59 1.11 1.6532 5 7 2 55.74 3.80 1.6493 12 11 0 55.81 4.34 1.6472 11 3 2 55.98 4.79 1.6426 6 13 0 56.12 3.86 1.6388 12 1 2 56.24 1.32 1.6356 18 4 1 56.29 1.91 1.6342 0 8 2 56.37 5.40 1.6321 6 7 2 56.40 3.72 1.6313 10 12 0 56.62 2.54 1.6257 12 2 2 56.64 1.87 1.6250 18 7 0 56.90 2.87 1.6182 6 12 1 56.90 4.88 1.6182 7 13 0 56.96 1.85 1.6167 11 4 2 57.03 2.80 1.6148 21 1 0 57.09 1.17 1.6134 16 9 0 57.29 1.22 1.6082 7 7 2 57.42 1.49 1.6049 4 8 2 57.43 8.96 1.6045 12 3 2 57.52 2.49 1.6023 21 2 0 57.70 1.94 1.5977 19 3 1 57.86 1.22 1.5938 14 9 1 57.88 1.43 1.5932 11 12 0 58.42 1.43 1.5798 11 5 2 58.51 2.50 1.5775 1 13 1 58.72 11.30 1.5725 2 13 1 59.06 4.72 1.5641 3 13 1 59.11 1.25 1.5628 1 9 2 59.16 1.48 1.5617 13 3 2 59.32 1.14 1.5579 2 9 2 59.37 1.63 1.5566 17 9 0 59.47 2.63 1.5542 18 6 1 59.59 2.91 1.5515 20 2 1 59.69 1.41 1.5490 7 8 2 59.85 3.75 1.5453 15 9 1 60.15 3.05 1.5383 5 13 1 60.27 1.09 1.5355 13 4 2 60.33 5.07 1.5341 6 14 0 60.38 2.56 1.5331 20 3 1 61.21 1.08 1.5142 7 14 0 61.57 1.80 1.5061 19 8 0 61.68 1.22 1.5038 13 5 2 61.89 5.18 1.4993 21 1 1 62.03 11.38 1.4961 0 10 2 62.09 1.46 1.4949 14 4 2 62.20 1.75 1.4925 11 7 2 62.93 1.67 1.4769 15 3 2 62.95 1.27 1.4766 2 14 1 63.12 4.51 1.4729 21 3 1 63.28 3.56 1.4697 3 14 1 63.36 1.15 1.4679 12 13 0 63.38 3.12 1.4676 13 6 2 63.72 5.96 1.4605 12 7 2 64.19 2.41 1.4509 21 4 1 64.24 1.67 1.4499 23 3 0 64.41 1.07 1.4466 6 10 2 64.46 1.24 1.4455 9 9 2 64.65 2.89 1.4416 18 10 0 64.85 2.41 1.4378 16 10 1 65.04 1.67 1.4339 6 14 1 65.30 1.35 1.4289 1 11 2 65.55 5.82 1.4241 21 5 1 65.69 1.72 1.4213 10 9 2 65.90 1.34 1.4174 17 1 2 65.99 2.65 1.4157 12 8 2 66.08 1.28 1.4139 24 1 0 66.50 1.29 1.4060 20 7 1 67.07 1.90 1.3955 0 15 1 67.36 1.63 1.3902 16 5 2 67.79 1.11 1.3823 18 11 0 67.98 3.20 1.3789 16 11 1 67.99 3.32 1.3788 18 0 2 68.28 1.19 1.3737 23 6 0 68.31 1.64 1.3731 24 4 0 68.51 1.45 1.3696 12 9 2 68.65 2.18 1.3671 5 15 1 68.66 1.77 1.3670 0 12 2 68.72 4.03 1.3660 5 16 0 69.11 7.39 1.3592 21 7 1 69.31 3.78 1.3557 18 3 2 69.40 3.33 1.3542 15 12 1 70.45 1.69 1.3365 11 14 1 70.90 1.84 1.3292 19 2 2 71.53 1.22 1.3191 2 3 3 71.63 1.48 1.3174 18 5 2 71.72 1.10 1.3159 7 12 2 71.84 2.43 1.3142 3 3 3 72.59 1.62 1.3024 4 16 1 72.78 2.95 1.2993 6 2 3 72.82 1.75 1.2988 5 3 3 72.84 1.91 1.2985 3 4 3 72.87 3.07 1.2980 11 11 2 73.02 3.26 1.2958 15 13 1 73.14 1.54 1.2938 5 16 1 73.73 1.89 1.2850 21 9 1 74.08 1.51 1.2799 8 1 3 74.28 2.46 1.2768 12 11 2 74.50 3.07 1.2736 6 13 2 74.73 1.16 1.2702 18 13 0 74.86 2.41 1.2684 10 12 2 74.92 3.17 1.2676 16 13 1 74.97 5.08 1.2668 9 0 3 75.06 1.31 1.2655 18 7 2 75.29 3.28 1.2622 7 13 2 75.40 1.80 1.2607 21 1 2 75.68 1.33 1.2566 3 6 3 75.82 1.56 1.2547 21 2 2 76.11 2.27 1.2507 4 6 3 76.69 2.03 1.2426 10 2 3 76.73 4.63 1.2421 26 1 1 76.84 4.30 1.2405 15 14 1 76.84 1.51 1.2405 3 17 1 76.92 1.06 1.2395 17 13 1 77.45 1.09 1.2324 17 9 2 77.51 4.51 1.2315 3 7 3 77.93 1.48 1.2259 4 7 3 78.30 3.72 1.2210 6 14 2 79.40 1.32 1.2069 19 8 2 81.80 1.28 1.1774 23 3 2 81.84 1.62 1.1770 13 16 1 82.18 2.26 1.1729 18 10 2 83.23 1.01 1.1608 27 5 1 83.49 1.05 1.1578 24 1 2 84.85 1.38 1.1428 15 3 3 85.55 1.41 1.1351 24 4 2 85.58 1.21 1.1348 16 1 3 85.81 3.65 1.1324 15 4 3 85.94 3.36 1.1310 5 16 2 85.98 1.93 1.1305 9 18 1 86.53 1.11 1.1248 27 7 1 88.55 1.15 1.1043 15 6 3 88.83 2.19 1.1016 9 10 3 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.