******************************************************************************
       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 Vladimirivanovite__R130034-9__Powder__Xray_Data_XY_RAW__11459[1]
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.026
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   17.4755 5.063228   0  1  7    2   17.4711  5.064494   -0.0044 -0.001265
   18.2137 4.859933   1  2  3    2   18.2163  4.859238    0.0026  0.000695
   22.7112 3.907751   2  0  5    2   22.7106  3.907858   -0.0006 -0.000107
   25.4023 3.499953   2  0  7    2   25.4005  3.500201   -0.0018 -0.000248
   25.9904 3.422154   1  1 10    2   26.0006  3.420830    0.0102  0.001323
   28.6075 3.115035   2  3  0    2   28.5943  3.116445   -0.0132 -0.001410
   32.2305 2.772944   2  0 11    2   32.2298  2.773000   -0.0007 -0.000056
   36.1340 2.482049   2  0 13    2   36.1348  2.481998    0.0008  0.000050
   42.8410 2.107948   4  1  6    2   42.8277  2.108571   -0.0133 -0.000622
   46.8296 1.937378   3  5  3    2   46.8252  1.937551   -0.0044 -0.000173
   55.2444 1.660672   2  6 12    2   55.2519  1.660465    0.0075  0.000208
   56.0540 1.638602   4  4 11    2   56.0653  1.638297    0.0113  0.000304
   58.6695 1.571663   4  4 13    2   58.6711  1.571624    0.0016  0.000040
   85.2673 1.136993   0  8 24    2   85.2633  1.137036   -0.0040 -0.000043

 rmse = 0.00007680768
 
     A =9.066(1)               B =12.875(2)               C =38.560(6)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 4500.8(5)