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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050217
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.013
  
 Number of iterations =   1

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   11.4042 7.761873   0  1  0    2   11.3988  7.765545   -0.0054 -0.003671
   12.4056 7.136799   1  1  0    2   12.4106  7.133949    0.0050  0.002850
   14.7345 6.012561   0  0  1    2   14.7390  6.010744    0.0045  0.001817
   20.3986 4.352932  -2 -1  1    2   20.3960  4.353483   -0.0026 -0.000551
   22.1303 4.015865  -1  1  1    2   22.1304  4.015841    0.0001  0.000023
   28.0504 3.179899   1  2  1    2   28.0502  3.179923   -0.0002 -0.000023
   29.7157 3.005294   0  0  2    2   29.7149  3.005372   -0.0008 -0.000078
   31.8264 2.810552  -1 -2  2    2   31.8266  2.810531    0.0002  0.000021
   34.6153 2.590138  -3 -3  1    2   34.6154  2.590128    0.0001  0.000010
   37.8059 2.378477  -3  0  2    2   37.8062  2.378458    0.0003  0.000019

 rmse = 0.00001580537
 
     A =8.969(3)               B =8.9714(9)               C =6.717(3)            
 Alpha =102.872(6)          Beta =116.51(6)           Gamma =59.95(3)            
 
 Volume = 418.6(0)