Umbite Ilyushin G D Izvestiya Akademii Nauk SSSR Neorganicheskie Materialy 29 (1993) 971-975 New data on the crystal structure of umbite K2ZrSi3O9*H2O _database_code_amcsd 0012738 CELL PARAMETERS: 10.2070 13.2410 7.1740 90.000 90.000 90.000 SPACE GROUP: P2_12_12_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 969.572 Density (g/cm3): 2.821 MAX. ABS. INTENSITY / VOLUME**2: 10.01875350 RIR: 1.157 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.94 43.70 8.0839 1 1 0 4 13.37 52.11 6.6205 0 2 0 2 14.04 5.05 6.3077 0 1 1 4 15.09 100.00 5.8693 1 0 1 4 16.52 10.82 5.3658 1 1 1 4 17.38 23.55 5.1035 2 0 0 2 18.23 10.47 4.8653 0 2 1 4 20.22 41.88 4.3919 1 2 1 4 21.37 4.20 4.1586 2 0 1 4 21.94 17.28 4.0511 1 3 0 4 22.41 3.45 3.9675 2 1 1 4 24.82 18.06 3.5870 0 0 2 2 25.25 16.17 3.5276 1 3 1 4 25.29 2.84 3.5215 2 2 1 4 25.73 8.01 3.4622 0 1 2 4 26.34 2.32 3.3841 1 0 2 4 26.70 2.73 3.3384 2 3 0 4 26.93 1.45 3.3103 0 4 0 2 27.06 32.68 3.2953 3 1 0 4 27.20 4.89 3.2787 1 1 2 4 28.30 2.41 3.1538 0 2 2 4 28.34 4.22 3.1488 1 4 0 4 29.05 31.74 3.0741 3 0 1 4 29.52 16.66 3.0261 3 2 0 4 29.65 17.20 3.0133 1 2 2 4 29.72 83.34 3.0057 0 4 1 4 29.84 27.12 2.9945 3 1 1 4 30.46 49.81 2.9346 2 0 2 4 31.02 29.35 2.8833 1 4 1 4 31.22 55.44 2.8651 2 1 2 4 32.10 6.30 2.7882 3 2 1 4 32.16 4.09 2.7836 0 3 2 4 32.23 12.45 2.7772 2 4 0 4 33.25 2.85 2.6946 3 3 0 4 33.36 7.62 2.6856 1 3 2 4 33.40 4.31 2.6829 2 2 2 4 34.63 10.81 2.5899 2 4 1 4 35.01 8.65 2.5633 1 5 0 4 35.59 16.18 2.5226 3 3 1 4 35.84 4.99 2.5056 4 1 0 4 36.78 1.69 2.4438 2 3 2 4 37.05 11.73 2.4267 3 1 2 4 37.41 6.17 2.4042 4 0 1 4 37.92 5.80 2.3726 3 4 0 4 38.03 6.24 2.3664 1 4 2 4 38.04 8.22 2.3655 4 1 1 4 38.25 2.08 2.3533 0 1 3 4 38.67 10.43 2.3283 1 0 3 4 38.94 2.68 2.3130 3 2 2 4 39.29 1.42 2.2931 1 1 3 4 39.89 1.46 2.2598 4 2 1 4 40.09 1.05 2.2491 0 2 3 4 40.38 10.22 2.2337 2 5 1 4 41.10 4.07 2.1964 1 2 3 4 41.10 3.06 2.1959 2 4 2 4 41.71 6.43 2.1654 2 0 3 4 41.88 11.06 2.1570 1 6 0 4 41.93 5.16 2.1544 3 3 2 4 42.29 2.75 2.1370 2 1 3 4 43.53 4.56 2.0793 4 0 2 4 43.83 2.00 2.0656 1 6 1 4 44.00 1.41 2.0581 2 2 3 4 44.09 12.91 2.0541 4 1 2 4 44.74 5.05 2.0256 2 6 0 4 45.19 9.75 2.0064 3 5 1 4 45.86 1.43 1.9789 3 4 2 4 46.17 1.55 1.9661 2 5 2 4 46.41 3.29 1.9564 3 0 3 4 46.59 8.15 1.9494 2 6 1 4 46.73 2.12 1.9440 2 3 3 4 46.77 3.14 1.9422 5 1 1 4 46.95 7.04 1.9354 3 1 3 4 47.76 1.42 1.9044 1 4 3 4 48.39 4.01 1.8810 4 3 2 4 48.43 2.49 1.8796 0 6 2 4 48.52 1.82 1.8762 3 2 3 4 48.97 1.78 1.8599 1 7 0 4 49.30 7.97 1.8485 1 6 2 4 50.35 13.10 1.8121 2 4 3 4 50.55 4.41 1.8057 3 5 2 4 50.71 1.37 1.8004 1 7 1 4 50.90 11.94 1.7940 5 3 1 4 50.91 4.09 1.7935 0 0 4 2 51.06 8.98 1.7886 3 3 3 4 51.33 15.14 1.7800 4 5 1 4 51.49 1.36 1.7748 0 5 3 4 51.75 1.67 1.7664 1 0 4 4 52.00 4.17 1.7585 5 1 2 4 52.25 3.96 1.7509 1 1 4 4 52.89 1.54 1.7311 0 2 4 4 53.20 3.13 1.7218 2 7 1 4 54.21 9.89 1.6921 2 0 4 4 54.37 6.84 1.6873 6 1 0 4 54.38 1.74 1.6873 4 2 3 4 54.48 2.45 1.6843 3 4 3 4 54.69 2.23 1.6784 2 1 4 4 54.76 9.83 1.6763 2 5 3 4 55.52 1.00 1.6553 6 0 1 4 55.52 3.16 1.6551 0 8 0 2 55.59 2.10 1.6532 3 7 0 4 55.67 1.98 1.6511 1 7 2 4 55.85 3.91 1.6462 5 3 2 4 55.99 3.87 1.6425 6 1 1 4 56.08 2.34 1.6400 1 3 4 4 56.25 2.68 1.6354 4 5 2 4 56.31 9.39 1.6338 1 8 0 4 56.73 1.98 1.6227 4 3 3 4 56.76 1.42 1.6218 0 6 3 4 57.54 2.30 1.6017 1 6 3 4 57.89 1.32 1.5930 1 8 1 4 58.53 1.08 1.5769 0 4 4 4 59.07 1.35 1.5638 5 4 2 4 59.30 3.26 1.5584 1 4 4 4 59.66 4.46 1.5499 6 3 1 4 59.84 2.94 1.5456 2 6 3 4 59.93 2.13 1.5436 4 4 3 4 59.99 7.36 1.5420 5 1 3 4 60.17 3.55 1.5378 2 8 1 4 60.21 1.63 1.5371 6 0 2 4 60.65 4.25 1.5268 6 1 2 4 61.25 1.29 1.5134 4 6 2 4 61.55 1.91 1.5066 2 4 4 4 61.79 4.48 1.5014 3 7 2 4 61.98 2.45 1.4972 6 2 2 4 62.46 4.51 1.4868 1 8 2 4 62.47 2.28 1.4866 4 7 1 4 62.76 1.49 1.4805 6 4 1 4 63.07 5.80 1.4740 5 5 2 4 63.35 1.77 1.4681 1 7 3 4 63.52 4.70 1.4646 5 3 3 4 63.82 3.86 1.4584 4 1 4 4 63.89 4.58 1.4570 4 5 3 4 64.16 2.20 1.4516 6 3 2 4 64.65 4.51 1.4416 2 8 2 4 65.46 1.06 1.4259 2 5 4 4 65.72 2.93 1.4208 1 0 5 4 66.14 2.68 1.4127 1 1 5 4 66.63 3.24 1.4036 6 5 1 4 67.00 2.90 1.3968 7 2 1 4 67.14 1.34 1.3941 6 4 2 4 67.24 1.82 1.3924 4 3 4 4 67.41 1.15 1.3892 1 2 5 4 67.51 3.70 1.3875 5 7 0 4 67.98 1.28 1.3791 1 6 4 4 68.22 3.02 1.3747 3 8 2 4 68.27 1.65 1.3738 2 1 5 4 69.00 1.31 1.3610 3 5 4 4 69.01 1.71 1.3609 0 8 3 4 69.09 2.70 1.3595 7 3 1 4 69.50 1.56 1.3525 1 3 5 4 69.69 1.14 1.3492 1 9 2 4 70.08 1.08 1.3428 2 6 4 4 70.28 1.03 1.3394 5 5 3 4 71.21 1.23 1.3242 6 6 1 4 71.69 1.65 1.3165 0 4 5 4 71.98 1.15 1.3119 7 4 1 4 72.38 1.75 1.3056 1 4 5 4 72.61 1.07 1.3021 0 10 1 4 73.13 3.49 1.2941 5 7 2 4 73.52 1.28 1.2882 3 6 4 4 73.83 1.27 1.2835 4 5 4 4 73.90 2.38 1.2825 4 7 3 4 74.16 1.56 1.2786 6 4 3 4 74.25 1.66 1.2773 7 5 0 4 74.35 1.25 1.2759 8 0 0 2 74.42 1.96 1.2747 2 4 5 4 74.44 2.03 1.2746 4 9 0 4 74.99 1.59 1.2665 3 3 5 4 75.34 3.00 1.2615 0 5 5 4 76.01 1.15 1.2520 1 5 5 4 77.76 1.17 1.2281 6 5 3 4 77.95 1.22 1.2257 8 3 0 4 78.02 1.38 1.2247 2 5 5 4 78.11 1.08 1.2235 7 2 3 4 78.64 1.10 1.2166 7 6 0 4 78.72 3.09 1.2156 3 7 4 4 79.33 2.38 1.2078 1 8 4 4 79.40 1.64 1.2069 2 10 2 4 79.71 1.60 1.2029 0 6 5 4 79.87 1.83 1.2010 4 9 2 4 79.88 1.24 1.2009 5 5 4 4 80.09 1.19 1.1982 7 3 3 4 82.05 1.74 1.1744 8 4 1 4 82.30 1.49 1.1716 2 11 0 4 82.94 1.28 1.1641 2 0 6 4 83.31 1.69 1.1598 8 3 2 4 83.67 1.05 1.1558 5 2 5 4 85.62 1.05 1.1344 5 3 5 4 86.29 1.00 1.1273 7 1 4 4 86.91 1.47 1.1209 3 11 1 4 87.18 1.37 1.1181 6 7 3 4 88.53 1.05 1.1045 9 2 1 4 89.06 1.52 1.0993 7 7 2 4 89.25 1.33 1.0974 5 7 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.