Priceite R050420

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Name: Priceite
RRUFF ID: R050420
Ideal Chemistry: Ca2B5O7(OH)5·H2O
Locality: 20-Mule-Team Canyon, Death Valley, California, USA
Source: Marcus Origlieri
Owner: RRUFF
Description: White cryptocrystalline massive
Status: The identification of this mineral has been confirmed by X-ray diffraction and chemical analysis
Quick search: [ All Priceite samples (2) ]
CHEMISTRY 
RRUFF ID: R050420.2
Sample Description: Microprobe Fragment
Measured Chemistry: Ca2.00B5.00O7(OH)5·H2O
Reference File: [ View PDF ]
RAMAN SPECTRUM 
RRUFF ID:
Sample Description: Unoriented sample
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Direction of polarization of laser relative to fiducial mark:
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BROAD SCAN WITH SPECTRAL ARTIFACTS
RRUFF ID: R050420
Wavelength:
Sample Description: Unoriented sample
Instrument settings: Thermo Almega XR 532nm @ 100% of 150mW
INFRARED SPECTRUM (Attenuated Total Reflectance) 
RRUFF ID: R050420.1
Instrument settings: SensIR Durascope on a Nicolet Magna 860 FTIR
Resolution:
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POWDER DIFFRACTION 
RRUFF ID: R050420.1
Sample Description: Powder
Cell Refinement Output: a: 11.6251(3)Å    b: 6.9773(3)Å    c: 12.3534(9)Å
alpha: 90.°    beta: 110.690(4)°    gamma: 90.°   Volume: 937.39(5)Å3    Crystal System: monoclinic
  File Type Information Close
Calculated diffraction file.

  File Type Information Close
Output file from the Bruker D8 Advance instrument. Includes device headers and XY data.

  File Type Information Close
Output file from the Bruker D8 Advance instrument. Includes device headers and XY data.

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REFERENCES for Priceite

American Mineralogist Crystal Structure Database Record: [view record]

Anthony J W, Bideaux R A, Bladh K W, and Nichols M C (1990) Handbook of Mineralogy, Mineral Data Publishing, Tucson Arizona, USA, by permission of the Mineralogical Society of America. [view file]

Silliman B (1873) Mineralogical notes on Utah, California and Nevada, with a description of priceite, a new borate of lime, American Journal of Science and Arts, 106, 126-133   [view file]

Foshag W F (1939) New mineral names, American Mineralogist, 24, 728-728   [view file]

Kramer H, Allen R D (1956) A restudy of bakerite, priceite, and veatchite, American Mineralogist, 41, 689-700   [view file]

Wallwork K S, Pring A, Taylor M R, Hunter B A (2002) The structure of priceite, a basic hydrated calcium borate, by ab initio powder-diffraction methods, The Canadian Mineralogist, 40, 1199-1206   [view file]

Sun W, Huang Y X, Li Z, Pan Y, Mi J X (2011) Hydrothermal synthesis and single-crystal X-ray structure refinement of three borates: sibirskite, parasibirskite and priceite, The Canadian Mineralogist, 49, 823-834   [view file]