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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050153
 
 Symmetry constraint is: TRICLINIC   
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.064
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    7.738111.510280   0  1  0    2    7.7408 11.506196    0.0027  0.004084
   10.0253 8.872026   1  0  0    2   10.0264  8.871083    0.0011  0.000942
   15.4540 5.752585   0  2  0    2   15.4526  5.753098   -0.0014 -0.000513
   16.9140 5.257292   1  0  1    2   16.9127  5.257685   -0.0013 -0.000392
   17.4464 5.097451   1 -1  1    2   17.4473  5.097183    0.0009  0.000268
   24.4261 3.650560   2  0  1    2   24.4261  3.650560    0.0000  0.000000
   28.1032 3.179619   0  3  1    2   28.1036  3.179575    0.0004  0.000043
   28.7417 3.110261  -1  3  1    2   28.7415  3.110282   -0.0002 -0.000020

 rmse = 0.00000773535
 
     A =     8.944(2)          B =    11.662(2)           C =     6.670(4)       
 Alpha =    95.88(2)        Beta =    90.49(5)        Gamma =    97.24(4)        
 
 Volume =    686.4(5)