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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050135
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.021
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    9.7378 9.094520   0  2  0    2    9.7428  9.089884    0.0050  0.004636
    9.9360 8.913169   0  0  2    2    9.9433  8.906649    0.0073  0.006520
   16.7734 5.287638   1  3  1    2   16.7744  5.287310    0.0010  0.000328
   17.0181 5.212063   1  1  3    2   17.0102  5.214480   -0.0079 -0.002417
   19.0927 4.649534   2  2  2    2   19.0937  4.649303    0.0010  0.000231
   20.7726 4.276787   3  1  1    2   20.7727  4.276772    0.0001  0.000015
   21.9535 4.049114   1  3  3    2   21.9516  4.049459   -0.0019 -0.000345
   22.2285 3.999592   0  2  4    2   22.2309  3.999167    0.0024  0.000424
   23.8712 3.727710   2  0  4    2   23.8733  3.727382    0.0021  0.000327
   26.3140 3.386664   1  1  5    2   26.3159  3.386419    0.0019  0.000245
   28.8024 3.099269   3  3  3    2   28.7999  3.099535   -0.0025 -0.000266
   29.5452 3.022964   1  5  3    2   29.5403  3.023460   -0.0049 -0.000496
   32.3278 2.768667   2  6  0    2   32.3308  2.768416    0.0030  0.000251
   35.0317 2.560788   3  5  3    2   35.0325  2.560734    0.0008  0.000053

 rmse = 0.00002024439
 
     A =    13.622(2)          B =    18.179(1)           C =    17.813(2)       
 Alpha =    90.             Beta =    90.             Gamma =    90.             
 
 Volume =   4411.6(5)