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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070249
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.018
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   15.7413 5.631303   1  1  0    2   15.7430  5.630683    0.0017  0.000620
   20.1231 4.412818  -1  1  2    2   20.1237  4.412686    0.0006  0.000132
   22.8012 3.899809   0  2  0    2   22.7972  3.900486   -0.0040 -0.000677
   25.4795 3.495340   2  1  1    2   25.4782  3.495509   -0.0013 -0.000169
   29.7405 3.003243   1  1  4    2   29.7451  3.002789    0.0046  0.000453
   31.1581 2.869683  -2  1  3    2   31.1590  2.869603    0.0009  0.000080
   34.2506 2.617189   2  2  2    2   34.2553  2.616839    0.0047  0.000351
   35.9374 2.498059   1  2  4    2   35.9320  2.498422   -0.0054 -0.000364
   37.9980 2.367131   0  0  6    2   38.0008  2.366966    0.0028  0.000165
   38.4818 2.338463   1  3  2    2   38.4798  2.338579   -0.0020 -0.000116
   39.5261 2.279025   0  3  3    2   39.5243  2.279124   -0.0018 -0.000099
   39.7846 2.264804   0  1  6    2   39.7810  2.264999   -0.0036 -0.000195
   41.3660 2.181765   1  1  6    2   41.3664  2.181745    0.0004  0.000020
   41.6932 2.165388  -2  3  1    2   41.6931  2.165396   -0.0001 -0.000007
   46.5483 1.950125   0  4  0    2   46.5453  1.950243   -0.0030 -0.000118
   54.8483 1.672930  -1  4  4    2   54.8494  1.672898    0.0011  0.000032
   57.8908 1.592009   4  3  1    2   57.8962  1.591872    0.0054  0.000137
   59.4288 1.554415  -5  1  2    2   59.4307  1.554368    0.0019  0.000046
   69.2550 1.355859   6  0  0    2   69.2513  1.355923   -0.0037 -0.000064
   73.0323 1.294750   0  6  1    2   73.0325  1.294748    0.0002  0.000003

 rmse = 0.00003251465
 
     A =8.1355(2)              B =7.8010(2)               C =14.2018(7)          
 Alpha =90                  Beta =90.028(7)           Gamma =90                  
 
 Volume = 901.32(5)