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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R070187
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.007
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
    5.570615.831742   0  1  1    2    5.5662 15.844190   -0.0044 -0.012448
    8.435010.465288   0  0  2    2    8.4415 10.457215    0.0065  0.008074
    9.1870 9.610921   0  1  2    2    9.1938  9.603868    0.0068  0.007054
   11.1435 7.928562   0  2  2    2   11.1526  7.922095    0.0091  0.006467
   14.6358 6.044512   0  2  3    2   14.6343  6.045121   -0.0015 -0.000609
   17.9043 4.948179  -1  1  3    2   17.9020  4.948802   -0.0023 -0.000623
   18.4503 4.803015   0  2  4    2   18.4545  4.801934    0.0042  0.001081
   19.2865 4.596692   1  3  1    2   19.2872  4.596529    0.0007  0.000163
   20.6414 4.298024   1  4  0    2   20.6394  4.298428   -0.0020 -0.000404
   22.4597 3.954113   0  2  5    2   22.4569  3.954598   -0.0028 -0.000485
   23.5600 3.771933   0  6  2    2   23.5533  3.772993   -0.0067 -0.001060
   25.4261 3.499246   0  6  3    2   25.4277  3.499031    0.0016  0.000216
   33.3859 2.681095  -1  8  2    2   33.3880  2.680930    0.0021  0.000165

 rmse = 0.00002107272
 
     A =6.189(1)               B =24.273(2)               C =21.256(3)           
 Alpha =90                  Beta =100.28(2)           Gamma =90                  
 
 Volume = 3141.9(8)