Boleite Diffraction data computed using the structure from the paper listed below, along with the cell parameters refined from the powder pattern of R050022 Cooper M A, Hawthorne F C The Canadian Mineralogist 38 (2000) 801-808 Boleite: Resolution of the formula, KPb26Ag9Cu24Cl62(OH)48 CELL PARAMETERS: 15.2890 15.2890 15.2890 90.000 90.000 90.000 SPACE GROUP: Pm-3m ATOM X Y Z OCCUPANCY ISO(B) K 0.50000 0.50000 0.50000 1.000 3.774 Pb 0.22633 0.50000 0.50000 1.000 1.674 Pb 0.30301 0.30301 0.30301 1.000 1.366 Pb 0.27356 0.50000 0.00000 1.000 1.848 Ag 0.00000 0.15730 0.00000 1.000 2.574 Ag 0.00000 0.50000 0.00000 1.000 3.103 Cu 0.25567 0.25567 0.09458 1.000 1.003 Cl 0.12220 0.12220 0.12220 1.000 2.345 Cl 0.38480 0.38480 0.12100 1.000 1.698 Cl 0.00000 0.32960 0.00000 1.000 1.848 Cl 0.13160 0.50000 0.13160 1.000 1.563 Cl 0.33060 0.50000 0.33060 1.000 2.574 O 0.00000 0.33020 0.21040 1.000 1.113 O 0.18800 0.18800 0.31190 1.000 1.390 H 0.00000 0.33900 0.14700 1.000 2.148 H 0.16200 0.16200 0.36400 1.000 4.035 X-RAY WAVELENGTH: 1.541838 BOUNDS ON TWO THETA: 5.0 90.0 LIMITS IMPOSED ON THE INDICES ARE: +/- 14 +/- 14 +/- 14 MAX. ABS. INTENSITY / VOLUME**2: 64.67085365 The INTENSITY cut off value is 1.00 2-THETA INTENSITY D-SPACING H K L 5.78 6.10 15.2890 1 0 0 10.02 7.16 8.8271 1 1 1 11.58 1.15 7.6445 2 0 0 12.95 3.27 6.8374 2 1 0 14.19 2.07 6.2417 2 1 1 16.40 3.32 5.4055 2 2 0 17.40 30.06 5.0963 2 2 1 17.40 9.07 5.0963 3 0 0 18.35 11.46 4.8348 3 1 0 19.25 4.93 4.6098 3 1 1 20.12 100.00 4.4136 2 2 2 20.95 11.53 4.2404 3 2 0 21.75 7.87 4.0862 3 2 1 23.27 74.26 3.8222 4 0 0 24.00 17.66 3.7081 3 2 2 24.71 7.80 3.6037 3 3 0 24.71 1.98 3.6037 4 1 1 25.39 35.36 3.5075 3 3 1 26.06 6.82 3.4187 4 2 0 26.72 9.64 3.3363 4 2 1 27.36 1.53 3.2596 3 3 2 28.60 31.79 3.1209 4 2 2 29.21 22.00 3.0578 5 0 0 29.80 7.23 2.9984 4 3 1 30.38 15.71 2.9424 3 3 3 31.51 21.91 2.8391 5 2 0 31.51 1.05 2.8391 4 3 2 32.06 3.16 2.7914 5 2 1 33.15 60.49 2.7027 4 4 0 33.68 6.12 2.6615 5 2 2 33.68 4.90 2.6615 4 4 1 34.20 13.87 2.6220 5 3 0 34.71 21.50 2.5843 5 3 1 35.22 22.93 2.5482 4 4 2 35.22 11.77 2.5482 6 0 0 36.22 3.95 2.4802 6 1 1 36.22 11.26 2.4802 5 3 2 37.67 21.83 2.3877 6 2 1 37.67 14.30 2.3877 5 4 0 37.67 5.58 2.3877 4 4 3 38.15 7.86 2.3591 5 4 1 38.62 33.61 2.3316 5 3 3 39.08 24.66 2.3049 6 2 2 39.54 3.99 2.2791 6 3 0 39.54 1.17 2.2791 5 4 2 40.89 1.31 2.2068 4 4 4 41.34 1.06 2.1841 6 3 2 41.34 1.74 2.1841 7 0 0 41.78 10.47 2.1622 5 4 3 41.78 3.20 2.1622 5 5 0 42.21 5.38 2.1409 5 5 1 42.21 1.16 2.1409 7 1 1 42.64 11.57 2.1202 6 4 0 43.07 1.02 2.1001 6 4 1 43.50 1.99 2.0806 6 3 3 43.50 10.39 2.0806 5 5 2 43.50 6.38 2.0806 7 2 1 44.34 5.04 2.0431 6 4 2 44.75 6.91 2.0251 7 2 2 44.75 7.94 2.0251 5 4 4 45.16 2.30 2.0075 7 3 0 45.57 9.98 1.9905 5 5 3 45.57 21.37 1.9905 7 3 1 46.38 1.85 1.9576 6 4 3 46.79 1.32 1.9417 6 5 1 47.58 10.42 1.9111 8 0 0 47.97 1.17 1.8964 6 5 2 48.36 1.38 1.8819 5 5 4 48.75 4.72 1.8678 7 3 3 49.14 5.20 1.8541 6 4 4 49.14 7.89 1.8541 8 2 0 50.66 10.55 1.8018 6 6 0 50.66 17.07 1.8018 8 2 2 51.04 5.35 1.7894 8 3 0 51.04 2.91 1.7894 6 6 1 51.41 2.72 1.7773 7 5 0 52.15 17.34 1.7538 6 6 2 52.52 3.15 1.7423 8 3 2 52.89 6.25 1.7311 7 5 2 53.62 4.09 1.7094 8 4 0 53.98 2.34 1.6988 6 6 3 53.98 1.75 1.6988 7 4 4 54.34 1.16 1.6884 9 1 0 54.69 4.06 1.6782 9 1 1 54.69 8.28 1.6782 7 5 3 55.05 3.18 1.6682 8 4 2 55.40 1.95 1.6583 7 6 0 55.76 1.87 1.6487 7 6 1 56.81 2.46 1.6206 8 4 3 56.81 1.35 1.6206 7 6 2 57.16 3.49 1.6116 8 5 1 57.16 1.35 1.6116 7 5 4 58.19 1.12 1.5854 8 5 2 58.53 2.44 1.5769 7 6 3 59.21 6.08 1.5604 8 4 4 59.89 2.24 1.5444 9 4 1 59.89 1.63 1.5444 8 5 3 59.89 1.03 1.5444 7 7 0 60.23 4.95 1.5366 7 7 1 60.23 4.33 1.5366 7 5 5 60.56 5.91 1.5289 10 0 0 60.89 3.55 1.5213 9 4 2 60.89 1.53 1.5213 7 6 4 60.89 1.18 1.5213 10 1 0 61.89 2.41 1.4992 10 2 0 62.22 1.66 1.4921 8 5 4 62.22 1.93 1.4921 10 2 1 62.55 1.11 1.4850 9 4 3 62.88 3.41 1.4780 9 5 1 62.88 3.45 1.4780 7 7 3 63.20 1.32 1.4712 6 6 6 63.53 1.68 1.4644 10 3 0 63.85 1.50 1.4577 9 5 2 64.82 1.26 1.4383 9 4 4 64.82 1.73 1.4383 10 3 2 65.15 2.94 1.4319 8 5 5 65.47 4.04 1.4257 9 5 3 65.79 4.60 1.4195 10 4 0 66.11 5.78 1.4135 8 7 2 66.11 2.56 1.4135 10 4 1 66.42 1.00 1.4075 10 3 3 67.06 4.12 1.3957 10 4 2 67.37 1.36 1.3899 7 6 6 67.69 2.09 1.3842 9 5 4 68.00 3.70 1.3786 7 7 5 68.00 1.19 1.3786 11 1 1 68.63 1.73 1.3675 8 6 5 68.63 1.52 1.3675 10 5 0 69.57 9.81 1.3514 8 8 0 70.50 4.87 1.3358 9 5 5 70.50 1.88 1.3358 11 3 1 70.81 7.25 1.3307 10 4 4 71.42 1.42 1.3208 11 3 2 71.42 2.05 1.3208 7 7 6 71.42 3.55 1.3208 10 5 3 72.03 2.60 1.3110 10 6 0 72.95 8.27 1.2968 11 3 3 72.95 1.26 1.2968 9 7 3 73.26 5.35 1.2922 10 6 2 74.77 1.06 1.2697 10 6 3 75.07 1.14 1.2653 9 8 1 75.98 1.38 1.2525 10 7 0 76.87 3.92 1.2401 12 2 2 77.17 2.63 1.2360 8 8 5 78.37 1.92 1.2202 12 3 2 78.66 1.47 1.2163 10 7 3 79.26 4.47 1.2087 12 4 0 79.55 3.00 1.2049 11 6 2 80.15 2.65 1.1975 9 9 1 82.21 1.04 1.1726 9 8 5 82.50 2.44 1.1692 11 7 1 83.09 1.23 1.1624 10 8 3 83.38 1.40 1.1591 11 7 2 84.85 7.05 1.1428 11 7 3 85.73 1.19 1.1333 11 6 5 87.19 1.29 1.1180 9 9 5 89.23 1.02 1.0977 12 7 1 89.52 5.35 1.0949 13 5 1 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.