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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 R050319
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.020
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   15.3380 5.779564   0  1  1    2   15.3361  5.780288   -0.0019 -0.000724
   15.9237 5.568008   2  0  0    2   15.9245  5.567721    0.0008  0.000287
   16.5261 5.366131  -1  1  1    2   16.5243  5.366715   -0.0018 -0.000583
   17.4973 5.070065   0  2  0    2   17.4976  5.069993    0.0003  0.000073
   18.0237 4.922993   1  1  1    2   18.0253  4.922572    0.0016  0.000421
   19.2403 4.614034   1  2  0    2   19.2395  4.614235   -0.0008 -0.000200
   20.9556 4.239708  -2  1  1    2   20.9571  4.239412    0.0015  0.000296
   23.3193 3.814663   2  1  1    2   23.3220  3.814235    0.0027  0.000429
   23.7396 3.748012   2  2  0    2   23.7354  3.748665   -0.0042 -0.000653
   25.5562 3.485353   3  1  0    2   25.5542  3.485620   -0.0020 -0.000268
   27.1505 3.284049  -3  1  1    2   27.1457  3.284618   -0.0048 -0.000569
   28.2196 3.161927  -2  0  2    2   28.2132  3.162628   -0.0064 -0.000701
   31.1339 2.872086  -1  2  2    2   31.1347  2.872009    0.0008  0.000076
   31.7787 2.815229   2  0  2    2   31.7780  2.815285   -0.0007 -0.000056
   32.1538 2.783217   4  0  0    2   32.1462  2.783860   -0.0076 -0.000643
   33.3853 2.683250  -2  2  2    2   33.3839  2.683357   -0.0014 -0.000107
   34.3210 2.612164   2  3  1    2   34.3196  2.612270   -0.0014 -0.000106
   36.3342 2.471835   1  4  0    2   36.3354  2.471756    0.0012  0.000079
   38.5592 2.334091  -4  0  2    2   38.5705  2.333434    0.0113  0.000657
   40.7448 2.213728  -2  1  3    2   40.7571  2.213090    0.0123  0.000638
   42.7499 2.114374  -4  3  1    2   42.7489  2.114423   -0.0010 -0.000049
   44.1609 2.050004  -1  4  2    2   44.1601  2.050038   -0.0008 -0.000034
   45.1239 2.008447   5  1  1    2   45.1253  2.008390    0.0014  0.000057
   45.8577 1.977987  -2  4  2    2   45.8573  1.978006   -0.0004 -0.000018
   46.9893 1.932936  -1  3  3    2   46.9856  1.933079   -0.0037 -0.000142
   47.6635 1.907145   4  2  2    2   47.6642  1.907117    0.0007  0.000027
   54.2500 1.690037   0  6  0    2   54.2514  1.689998    0.0014  0.000039
   58.3266 1.581206  -4  0  4    2   58.3222  1.581314   -0.0044 -0.000108
   59.1588 1.560926   6  0  2    2   59.1591  1.560919    0.0003  0.000007

 rmse = 0.00003900892
 
     A =11.2282(7)             B =10.1400(4)              C =7.0939(4)           
 Alpha =90                  Beta =97.368(4)           Gamma =90                  
 
 Volume = 800.99(5)