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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R060292
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.004
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   32.3475 2.765644  -2  0  6    2   32.3406  2.766218   -0.0069 -0.000574
   38.5637 2.332894   0  2  4    2   38.5591  2.333159   -0.0046 -0.000265
   42.6582 2.117949   2  2  3    2   42.6550  2.118101   -0.0032 -0.000152
   45.6943 1.984023   3  1  5    2   45.6923  1.984106   -0.0020 -0.000083
   53.7818 1.703174   3  1  7    2   53.7814  1.703185   -0.0004 -0.000011
   30.1287 2.964099   0  0  6    2   30.1295  2.964021    0.0008  0.000078
   19.9568 4.446254   0  0  4    2   19.9578  4.446032    0.0010  0.000222
   39.9948 2.252647  -4  0  4    2   39.9970  2.252528    0.0022  0.000119
   36.5127 2.459107   3  1  2    2   36.5153  2.458935    0.0026  0.000172
   28.9593 3.081093   1  1  4    2   28.9644  3.080561    0.0051  0.000533
   45.0089 2.012633   0  2  6    2   45.0152  2.012366    0.0063  0.000267

 rmse = 0.00004281999
 
     A =9.473(1)               B =5.4818(6)               C =18.165(2)           
 Alpha =90                  Beta =101.755(7)          Gamma =90                  
 
 Volume = 923.5(0)