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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
 ******************************************************************************
 
 SamarskiteY__R070161-1__Powder__Xray_Data_XY_Processed__9657[1]
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.004
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   24.3551 3.651110   1  1  0    2   24.3412  3.653167   -0.0139 -0.002058
   30.0962 2.966505   1  1  1    2   30.0984  2.966293    0.0022  0.000212
   31.2260 2.861712   2  0  0    2   31.2437  2.860135    0.0177  0.001577
   37.8791 2.373020   0  2  0    2   37.8679  2.373699   -0.0112 -0.000678
   43.3464 2.085557   1  1  2    2   43.3366  2.086006   -0.0098 -0.000449
   49.8743 1.826818   2  2  0    2   49.8812  1.826584    0.0069  0.000235
   51.6118 1.769332   3  1  0    2   51.6104  1.769375   -0.0014 -0.000044
   52.7307 1.734395   0  2  2    2   52.7244  1.734588   -0.0063 -0.000193
   53.2449 1.718852   2  2  1    2   53.2425  1.718925   -0.0024 -0.000073
   60.1607 1.536749   1  1  3    2   60.1581  1.536810   -0.0026 -0.000060
   62.5536 1.483594   2  2  2    2   62.5746  1.483146    0.0210  0.000448
   80.6106 1.190757   4  2  1    2   80.6042  1.190835   -0.0064 -0.000078

 rmse = 0.00012611358
 
     A =5.7203(8)              B =4.7474(9)               C =5.0820(8)           
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 138.01(2)