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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050028
 
 Symmetry constraint is: ORTHORHOMBIC
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:    0.005
  
         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   15.3378 5.770231   1  0  1    2   15.3335  5.771837   -0.0043 -0.001605
   21.5908 4.111542   1  1  1    2   21.5876  4.112149   -0.0032 -0.000607
   22.8121 3.894157   1  0  2    2   22.8216  3.892562    0.0095  0.001595
   25.8159 3.447549   2  0  1    2   25.8086  3.448504   -0.0073 -0.000955
   30.9624 2.885327   2  0  2    2   30.9559  2.885918   -0.0065 -0.000592
   34.2685 2.614188   1  2  1    2   34.2890  2.612671    0.0205  0.001518
   34.6132 2.588943   2  1  2    2   34.6125  2.588994   -0.0007 -0.000051
   44.0153 2.055335   2  2  2    2   43.9986  2.056075   -0.0167 -0.000740
   49.8309 1.828254   3  1  3    2   49.8398  1.827949    0.0089  0.000305
   50.6462 1.800722   0  2  4    2   50.6445  1.800777   -0.0017 -0.000055

 rmse = 0.00010443729
 
     A =7.449(2)               B =5.860(2)                C =9.131(3)            
 Alpha =90                  Beta =90                  Gamma =90                  
 
 Volume = 398.6(0)