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       **Program REFINE Version 3.0**  Kurt Bartelmehs and Bob Downs, 1998
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 R050469
 
 Symmetry constraint is: MONOCLINIC2 
 
 Wavelength #1 =  1.541838
 Wavelength #2 =  1.540562
 Wavelength #3 =  1.544390
 
 Refinement after correcting for machine error
  
 MACHINE ERROR:   -0.045
  
 Number of iterations =   0

         OBSERVED                         CALCULATED          DIFFERENCE
    2theta      d     h  k  l  Wave#  2theta       d      2theta       d
   16.2311 5.471619   0  1  1    2   16.2116  5.478187   -0.0195 -0.006567
   18.4693 4.811643   0  1  2    2   18.4776  4.809482    0.0083  0.002160
   19.3028 4.605223   1  0  0    2   19.3078  4.604031    0.0050  0.001192
   25.1637 3.542381  -1  1  1    2   25.1571  3.543297   -0.0066 -0.000916
   27.7390 3.218537  -1  0  4    2   27.7541  3.216812    0.0151  0.001725
   29.5828 3.021689   1  1  3    2   29.5755  3.022415   -0.0073 -0.000726
   35.4241 2.535021  -1  1  5    2   35.4158  2.535599   -0.0083 -0.000578
   36.0523 2.492221  -1  0  6    2   36.0534  2.492149    0.0011  0.000072
   36.3976 2.469336   1  1  5    2   36.4000  2.469177    0.0024  0.000159
   39.1434 2.302007   2  0  0    2   39.1433  2.302016   -0.0001 -0.000008
   39.4644 2.283998   0  1  7    2   39.4848  2.282866    0.0204  0.001132
   41.5472 2.174058   0  0  8    2   41.5313  2.174855   -0.0159 -0.000797
   59.4419 1.554766   2  0  8    2   59.4424  1.554755    0.0005  0.000011
   82.7525 1.165850  -3  2  8    2   82.7524  1.165851   -0.0001 -0.000001

 rmse = 0.00009458749
 
     A =4.6067(7)              B =5.772(4)                C =17.409(3)           
 Alpha =90                  Beta =91.95(1)            Gamma =90                  
 
 Volume = 462.6(0)